Setline synchronous thermal analyzer

Synchronous thermal analyzerSetline STA

4000686368

Instrument Introduction

The headquarters of the French Kaipu Technology Group is located in Lyon, France, with60The research and production history of annual thermal analysis instruments, and their products have numerous applications in the fields of high temperature, ultra-high temperature thermal analysis, and calorimetry.Setline STA/STA⁺The series of synchronous thermal analysis products is a joint venture product under its umbrella.2018Released in China in the year, this series of products includes the Setline DSC differential scanning calorimeterandSynchronous thermal analyzerSetline STAFour products from two series. brand newSetline®The platform has invested the joint efforts of Chinese, French, and Swiss R&D teams, adopting a collaborative approach of European R&D, procurement, and local production, which can bring users superior performanceProducts, flexible customized services, and multi-faceted approachesPre sales and after-sales service experience.

Setline STAWhether in terms of production process, raw material control, software matching, or instrument performance indicators, it is equivalent to the original factory level. Under the condition of greatly reducing costs, it truly eliminates the generation gap between Chinese manufacturing and European and American products in terms of process level, technical means, and performance.Setline®Series as a new generation universal modelDSC/STACreated precisionA new era of localization of thermal analyzers!

futureSetlineThe series of products will focus on segmented markets such as universities, research institutes, enterprise technology research and development, and quality inspection centers, injecting new vitality into domestic scientific research and production.

easy to use

l Setline® STA/STA +Easy to operate, suitable for various educational andQCWaiting for application fields;

l He adopts a reasonable design, is sturdy and durable, can obtain stable signals, and performs accurate and reliable measurements.

l DSCSensor technology ensures excellent data quality and guarantees the repeatability and reliability of experimental data.

l Setline®Compact design, powerful functionality, and space saving;

l Accessories focused on core requirements ensure quick mastery and ease of use;

l Setline®（STA+）Configure an automatic sampler to handle multiple experiments.

Easy maintenance

l Setline®Specially designed to ensure durability under continuous use conditions;

l By simplifying the maintenance process and allowing for individual replacement of certain components as needed, the cost of use is greatly reduced;

l Setline®The technical and application support can provide fast and professional assistance.

l SwitzerlandCalisto 2.0Professional thermal analysis software ensures intuitive and convenient operation of the instrument.

powerful

CalistoCan process any thermal analysis data from any instrument or brand, suitable for allSetaramThe instrument consists of two independent parts:

l CALISTOData collection software dedicated toSetline® STA/STA+Control and Data Collection

l CALISTOData processing software is used forSetline® STA/STA+Data Processing

Technical Features

TG/DSC/DTASynchronous sensor

Setline STA/STA +ofTG/DSC/DTAThe synchronous sensor adopts a hot flow flat plate design to ensure full temperature range

Range (room temperature)~1100It can maintain ultra-high sensitivity within (℃).

High precision photoelectric balance

All using FranceSETARAMProud of its high-precision photoelectric balance technology, inheriting its powerful technology

Gene, balance resolution can reach0.02ugCan provide * sensitivity and reliability.

Flexible and variable crucible

Synchronize with the French headquarters,SETARAMChina can provide a variety of sample crucibles (made of materials such as aluminum, aluminum oxide, platinum, gold-plated, stainless steel high-pressure, etc.) according to different application needs.

SwitzerlandCalisto 2.0Professional thermal analysis software

cooperate, coordinate, collaborateCalistoSoftware,Setline® STAandSTA +Not only is it easy to operate, but it also has powerful functions.CalistoCan process any thermal analysis data from any instrument or brand, suitable for allSetaramThe instrument consists of two independent parts:

l CALISTOData collection software dedicated toSetline® STA/STA+The control and data collection, including intuitive experimental program settings, can be saved and reapplied to other sample tests.

l CALISTOData processing software is used forSetline® STA/STA+Data processing, including:

- Powerful heat effect processing function (single and multiple mass changes, residual mass,DTGDeducting blanks,DSCPoints, etc.)

- Data integrity function with user permission management options, traceable and securely accessible data modifications, etc;

- According to the requirements, use user recorded macros to automatically process data;

- Can present the most influential data;

- Export directly to graphic or spreadsheet format.

Setline synchronous thermal analyzerSTA Technical Parameters

Application field

Setline® STAandSTA+The simplicity and powerful functionality make it a preferred instrument for thermal analysis,Setline® STAandSTA +Mainly used for measuring:

l The thermal stability, thermal aging, and decomposition of most materials

-Polymers, elastomers, drugs, biomaterials, organic compounds such as coal, oil, lubricants, etc

l Research on Thermal Effect:

-Pyrolysis, combustion

-desorption

-Dehydration and dehydroxylation

l Component analysis:

-Ash content, carbon content, filler content, and additive content

-Moisture and solvent content

Application Cases

Component analysis of rubber samples

Analyze the components of rubber samples of different qualities. Heat the sample in two steps under inert gas flow (nitrogen) until700℃, cool to400℃ and reheat to900℃ and switch the atmosphere to air.TGThe two mass losses of the curve correspond to plasticizers and elastomers（i）And carbon black（ii）The decomposition. The remaining mass after the experiment corresponds to the rubber（iii）The ash content. According to the test results（i）In57.7and67.7%Between changes（ii）In4.5and5.8%Between changes, and（iii）In19.9and29.6%Changes between them. Due to pre recorded macros, they can be automatically processed12A quality loss.

Determination of free water content in drugs

Measure the free water content of three different batches of drugs using quality change signals. The endothermic heat flux signal can determine the temperature range of free water release. Due to pre recorded macros, quality loss and heat absorption peaks can be automatically processed.

Calcium oxalate monohydrate（CaC2O4，H2O）Sample measurement

Through quality loss（TG）And heat flow（DSC）Measurement of Calcium Oxalate Monohydrate（CaC2O4，H2O）Sample. From low temperature to high temperature: dehydration, formation of calcium carbonate, and formation of calcium oxide. This simple case highlights the application of thermogravimetric analysis in quantitative measurement. This also demonstratesSTAThe method is used to identify the thermal decomposition process of materials and detect the effects of heat absorption or release.

Analyze the components of synthetic rubber

Analyze the components of synthetic rubber. In an inert atmosphere（N2）Heat the sample in two steps to600After cooling to ℃400℃, and switch the atmosphere to air. After holding for a period of time, heat the sample to800°C.TGThe curve has three mass losses corresponding to the decomposition of plasticizers: oil and wax content（3.6%), elastic content（57.9%) and carbon black content（38.7%). The remaining mass at the end of the experiment corresponds to the ash content of the rubber, but it is not shown in this case（<0.5%).

Setline synchronous thermal analyzerSTA Warranty Service:

Warranty and Follow up

The instrument manufacturer provides a one-year warranty for the entire product sold from the date of installation and acceptance. During the warranty period, the instrument manufacturer shall appoint technical engineers to provide free maintenance, upkeep, and replacement of non-human damaged or defective parts for the buyer's equipment, and conduct regular follow-up visits to the buyer. After the equipment warranty period, the instrument manufacturer shall provide lifelong preferential technical support for the equipment.

Technical engineers shall visit the buyer at least once a year (for a period of no less than 10 years, in the form of on-site or telephone communication) to understand the use of the instrument and provide guidance.

Technical Support

Service support and consultation

Regularly provide instrument technology communication, hold technical lectures and user technical exchange activities every year; Establish an application laboratory in China and assist users in solving testing technology problems, providing targeted information according to user needs.

Instrument manufacturers allocate dedicated maintenance engineers. When the equipment malfunctions or cannot operate normally, the manufacturer provides 24-hour telephone consultation service.

Installation and debugging guarantee:

After receiving the user's notification to install the instrument, dispatch engineers to the user's site within two weeks to install and debug the instrument for free.

training

Dispatch engineers to be responsible for on-site technical training for users, training 2 or more people until they can operate independently, including basic operations, basic maintenance of instruments, and simple troubleshooting of instruments. After systematic training, experimental operators are able to independently operate and run instruments.

Training content

SetlineSTA installation and training within China, approximately 1 working day.

Open box inventory, installation, standard sample testing, and data analysis of STA equipment and components;

STA principle explanation, maintenance training, instrument application, experimental skills and precautions.

some clients:

China University of Petroleum

Beijing Jiaotong University

Shandong University of Science and Technology

School of Safety Engineering, Qingdao University of Science and Technology

Hebei University of Science and Technology

Shandong Shengbang Plastic Co., Ltd

Hebei University of Technology

Hebei Lansheng Biopharmaceutical Technology Co., Ltd

Xiamen Overseas Chinese University

Anhui Zhuji New Material Technology Co., Ltd

South China Normal University

Northeastern University

Anshan University of Science and Technology

Minkang Baicao Pharmaceutical Co., Ltd

Zaozhuang University

binzhou university

Linyi University

Liaoning University of Science and Technology

Jiefang Military Materials and Equipment Department

Linglong Tire

Department of Civil Engineering, Tsinghua University

University of Science and Technology of China

University of Jinan

Beijing University of Science and Technology

Dalian Kotian New Materials Co., Ltd

China University of Traditional Chinese Medicine

Zhejiang Hengyida Composite Materials Co., Ltd

China Aerospace Standardization Institute

Dalian Institute of Chemical Physics, Chinese Academy of Sciences

Jiangsu Xiannuo New Material Technology Co., Ltd

CNOOC Oilfield Services Co., Ltd

China National Petroleum Corporation Limited

Petrochemical Research Institute

For more information on Setaram thermal analysis and calorimetry products, as well as free basic knowledge and practical exercise manuals, please visit the Setaram website Setaram Solutions.