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PVC material torque rheometer

NegotiableUpdate on 12/22
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Overview
The PVC material torque rheometer consists of a mixing torque rheometer, an extrusion capillary rheometer, a capillary testing die, a data acquisition and measurement system, an electronic computer, and operating software. In the process of processing and forming materials, their flowability is almost always involved. For example, in processes such as extrusion, injection molding, blown film, and rolling, the flow behavior of materials is crucial. The fluidity of materials not only affects processing behavior, but also affects the mechanical properties of the final product. For example, molecular orientation has a significant impact on the mechanical properties of molded products, films, and fibers. The type and degree of molecular orientation are mainly determined by the processing process
Product Details

HZJ-300D pipe materialPVC materialHAAKE Polylab OS

1

PVC材料转矩流变仪

Overview

1.1Product Features

During the processing and molding of rubber and plastic materials, their flowability is almost always involved. For example, in processes such as extrusion, injection molding, blown film, and rolling, the flow behavior of materials is crucial. The fluidity of materials not only affects processing behavior, but also affects the mechanical properties of the final product. For example, molecular orientation has a significant impact on the mechanical properties of molded products, films, and fibers. The type and degree of molecular orientation are mainly determined by the characteristics of the flow field and the flow behavior of the material during the processing.

pipe materialPVC materialHAAKE Polylab OSIt's researchPVCMaterials andpolymerFlow of materialsWith deformationPlasticization and thermal shear stabilityDynamic rheological propertiesPlasticizing behavior and applying torque to the results--Time and torque--Ideal equipment represented in chart form for temperature and other parametersIt can be widely used in scientific research and production, and is an important instrument for conducting scientific research and guiding production. General instruments for studying material flowability——Compared to viscometers, this rheometer provides a dynamic measurement method that is closer to actual processing. It can continuously, accurately, and reliably measure the rheological properties of materials under conditions similar to actual processing, such as mixing of multi-component materials, crosslinking and curing of thermosetting resins, vulcanization of elastomers, dynamic stability of materials, and the influence of screw speed on the processing performance of the system.

1.2Scope of Application

pipe materialPVC materialHAAKE Polylab OSIt can be used to study the thermal stability, shear stability, flow and plasticization behavior of thermoplastic materials. Its biggest feature is that it can continuously, accurately and reliably measure the rheological properties of the system in a similar actual processing process. It can also complete the curing characteristics testing of thermosetting materials.

1.3Application field

1TheUPVCResearch on Processing Performance and Material Development

2Development and Processing Performance Research of Thermoplastic Materials

3Research on the curing properties of cross-linked and thermosetting resins

4Teaching and Research Applications

IIStructural features and working principle

1System composition

pipe materialPVC materialHAAKE Polylab OS

PVC材料转矩流变仪

It consists of a mixing torque rheometer, an extrusion capillary rheometer, a capillary testing die, a data acquisition and measurement system, an electronic computer, and operating software.

Internal torque rheometer:

pipe materialPVC materialHAAKE Polylab OSIt mainly consists of imported servo motors, high-precision dynamic torque sensors, gearboxes, mixing chambers, temperature modules, measurement modules, computers, measurement and control software, etc. Its principle is shown in the figure2As shown:

image1 Internal torque rheometer

A closed mixer is equivalent to a small internal mixer, consisting of a The detachable mixing chamber in the shape of an "∞" and a pair of rotors rotating in opposite directions at different speeds. In the mixing chamber, the rotors rotate in opposite directions, applying shear to the materials and forcing them to mix in the mixing chamber; The two rotors have different speeds, resulting in dispersed mixing in their gaps.

The overall appearance of this machine is beautiful, and the main sheet metal adopts a color scheme of milky white and blue, which can also be processed according to the user's color requirements. The stainless steel part adoptsSUS304stainless steel.

Computer software has functions for data collection, storage, calculation, analysis, and output, and can print test reports according to user requirements.



image2 secretsRefining torque rheometer image3 eachType rotor

PVC材料转矩流变仪


image4secretRefining styleSchematic diagram of torque rheometer

1- Compression rod;2- Feeding port;3- Mixing room;4- Leakage of materials;5- Internal mixer;6- Emergency brake switch;

7- Manual panel;8- Drive and torque sensors;9- Switch;10- Computer

PVC材料转矩流变仪


image5 Test curve of internal torque rheometer


PVCfusionPVCthermal stability

XLPEcrosslinkingPVCfusion

ØExtrusion capillary rheometer:

The extrusion capillary rheometer is mainly composed of imported servo motor, reducer, extrusion screw, die, measurement and control module, temperature module, pressure sensor, electronic computer and measurement and control software. The principle is that through the rotation of the screw, the animal material is carried throughoral modelExtrusion is the process of measuring the shear rate and shear pressure of a material, and calculating the viscosity of the material at a specified temperature. simultaneouslyThe extrusion capillary rheometer can also be used as an instrument for production process testing. By replacing different types of molds and using a small amount of material for actual production and processing, various methods such as controlling extrusion speed, melt temperature, and formula ratio are used to verify the production process.

The core part of an extrusion capillary rheometer is a set of delicate capillaries with different aspect ratios (usuallyL/D =10/120/130/140/1By conducting comparative experiments with different aspect ratios of mouth molds (keeping other conditions constant, such as temperature, etc.), different pressure values were obtained, and the viscosity of the material was calculated.

Capillary specifications

serial number

diameterD(mm)

Capillary lengthL(mm)

aspect ratioL/D

Remarks

1

1.27

25.4

20

markmatch

2

38.1

30

3

50.8

40

4

1.5

30

20

selectmatch

5

45

30

6

60

40

7

2.0

40

20

selectmatch

8

60

30

table1 oftenUsing capillary specifications

image6 Capillary die

This device is equipped with screws of different parameters that rotate inside a cylinder with a certain temperature, and a feeding hopper is located at the other end of the cylinder. When the raw materials are sent to the cylinder2/3The material gradually plasticizes and is homogenized in the remaining part of the cylinder. When all particles are melted, it can be extruded into a mother material using a capillary extrusion mold or injected into a mold for forming. At the same time, the equipment also measures the relationship between the material's apparent viscosity, shear rate, and shear stress.

extrudeMachines can choose different types based on the characteristics of different materialsScrew,The compression ratio of screws has a significant impact on the experimental performance of materials.screwCan be easily interchanged to support rapid testing of different materials.

image6 variousType of screw

IIIMain technical characteristicsAnd configuration

It can be used to study the thermal stability, shear stability, flow and plasticization behavior of thermoplastic materials. Its biggest feature is that it can continuously, accurately and reliably measure the rheological properties of the system in a similar actual processing process. It can also complete the curing characteristics testing of thermosetting materials.

1. Motor power: JapanPanasonic3.0kwwatch forService motor

2. Motor speed3000 rpm

3. motordrive3.0 kw

4. reduceSpeed generator120Import

5. Power output speed:0 ~ 150rpm

6. Speed control accuracy:0 .05%F.S

7. Temperature control:5Road temperature measurement, including4Road temperature control

8. Static measurement accuracy:0.1°C

9. Temperature control accuracy:±1°C

10. Torque measurement range:0 ~ 250Nm

11. Torque measurement accuracy:0.1%F.S

12. Measurement range of melt pressure:0.1 ~ 100 Mpa

13. Measurement accuracy of melt pressure:0.5%F.S

14. Software: Measurement and control software, polymer melt viscosity measurement data processing software, extruder data processing software, mixer data processing software.

15. Graphic display: speed, torque, temperature, pressure

16. Voltage:AC380V 7.5kw

The mixer platform can perform various experiments such as multi-component thermoplastic material thermal fusion testing, thermosetting material curing performance testing, thermal stability testing, shear sensitivity testing, material mixing, etc.

1. Rong Quantity:60ml 200ml (Optional)

2. material Quality:304L

3. Rotor type:Roller

4. Rotor processing: After high-precision polishing, the surface is chrome plated

5. turn quick Compared to:32

6. Maximum Torque250 Nm

7. maximum temperature:400

8. Temperature sensor:KClass thermocouple

9. Heating method: electric heating

10. Heater: Heating tube

11. Heating total power:1700W

12. Heating zone:3road

The twin-screw extruder unit is mainly used for filling, blending, modifying, reinforcing, chlorinated polypropylene and high water absorbing resin in rubber and engineering; Extrusion of biodegradable masterbatch, polyamide polymerization, polyurethane polymerization reaction, granulation of carbon powder and magnetic powder, insulation material and sheath material for cables, low smoke and low halogen flame retardant typePVCPreparation of cable materials and various silane crosslinking materials.

Plastic single screw extruder (material)38CrMOALA)(Optional, price negotiable)

1TheL:D 251

2Screw diameter: φ20mm

3Screw compression ratio: 2.51

4maximum temperature: 350

5Heating method: electric heating

6Heating zone: 5road

7Heating total power:4200W

8Temperature sensor:KClass thermocouple

9Machine volume (length)X Width x Height): 1600×450×1300mm

10Capillary mold:φ1.27 aspect ratio201301401One mold core each

φ1Theφ2Other specifications are optional, prices are negotiable

Cylindrical mold head (optional):inner diameterF5, outer diameterF10

Parallel and opposite direction twin-screw extruder (optional, price negotiable)

1Screw type: Parallel and opposite direction twin-screw

2Screw diameter:42mm

3Effective length of screw:276mm

4Effective length of screw tube:276mm

5Temperature range: room temperature~350

6Temperature control accuracy:±0.5%F.S

7Temperature sensor:KType thermocouple

8Heating total power:2500W

9Mold specifications:60×1.5mm

Main Configuration

serial number

constitute become

type number

quantity

manufacture make factory home

1

host

HZJ-300A

1 unit


Servo motor and driver

3.0kW

1 unit

JapanPanasonic

High precision gearbox

120

1 unit

Import

High precision torque sensor

300Nm

1 unit

joint venture

internal mixer

60mL

1 unit

self-produced

Temperature control module

Room temperature~350℃

1 set

self-produced

data acquisition module


1 set

Japan

High precision melt pressure sensor

0~100MPa

1 unit

Shanghai

twin screw

L/D =40/1

1 unit

self-produced

3

computer

Mouse, keyboard, data interface

1 unit

branded computer

4

Cleaning tools


2 sets

self-produced

hex key


1 set

market procurement

adjustable wrench


1 piece

market procurement

screwdriver


1 piece

market procurement

5

software packageExperimental software (adapted)Win 7 ,10

1set