Simpsil P-SAX Glyphosate Specific Column

NegotiableUpdate on 05/06

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Nature of the Manufacturer: Producers

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Overview

Simpsil P-SAX glyphosate specific column is a quaternized polyvinyl alcohol anion analysis column, 150mm 4.0mm (inner diameter), 5 μ m (particle size), it is a high-performance chromatographic column made of highly cross-linked quaternized polyvinyl alcohol as the matrix, bonded with anion exchange functional groups through our company's unique surface modification technology, which meets the standard requirements of "GB 23200.122-2026 National Food Safety Standard for Determination of Residues of Four Pesticides and Their Metabolites, including Glyphosate, in Plant derived Foods by Liquid Chromatography Mass Spectrometry".

Product Details

SimpSil P-SAXThe glyphosate specific column is a quaternized polyvinyl alcohol anion analysis column,150mm×4.0mm(Inner diameter),5Mm(Particle size), it is based on highly cross-linked quaternized polyvinyl alcohol as the matrix, and processed by our company's unique formulaSurface modification technology, high-performance chromatography column formed by bonding anion exchange functional groups, in compliance with《GB 23200.122-2026 National Food Safety Standard: Glyphosate in Plant Derived FoodsPhosphine, etc4 Determination of pesticide and its metabolite residues by liquid chromatographyscore-The standard requirements for mass spectrometry.

Activation of chromatographic columns

SimpSil P-SAXThe activation of glyphosate specific columns requires the use of80%Water is used for flushing, and the flow rate is generally set to1.0 mL/minRinse the chromatographic column at least5~ 10One column volume, and then switch to analyzing the mobile phase. Attention: The equilibrium time of ion exchange chromatography columns is relatively long and generally requires1~2Hour.

Flushing and preservation of chromatographic columns

P-SAXIt is recommended to store the glyphosate specific column in the mobile phase after use.

Solution for reducing column efficiency in chromatography

When abnormal phenomena such as increased column pressure, decreased column efficiency, abnormal peak shape, and decreased separation occur in the chromatographic column, maintenance of the chromatographic column is required:

Rinse program	0. 1%acetic acid0.3MPhosphates (containing 0. 1%Ethylenediaminetetraacetic acid,pH 7.0）0. 1%acetic acid
Rinse time	In sequence:20 min90 min20 min
flow speed	Sample flow rate
pillar warm	40℃

《GB 23200.122-2026 National Food Safety Standards Glyphosate and other compounds in plant-based foods 4 Determination of pesticide and its metabolite residues liquid chromatography-Excerpt from "Mass Spectrometry":

7.5determination

7.5.1Reference conditions for liquid chromatography

a）Chromatography column: quaternized polyvinyl alcohol anion analysis column,150mm×4.0mm(Inner diameter),5Mm(Particle size)Or equivalent.

b）Mobile phase:AAs water,BThe phase is ammonium bicarbonate-ammonia solution(4.2.4)The gradient conditions of the mobile phase are shown in the table1.

c）Flow rate:0.6 mL/min.

d）Column temperature:40℃。

e）Injection volume:10ML.