Research on the Intelligent Control TA03 Fully Automatic Reaction Calorimeter

Purpose and standards

1.A fully automatic reaction calorimeter is a professional testing instrument that simulates the specific process of chemical reactions on a liter scale and measures and controls important process variables. Carefully researched and developed through multi-faceted market research and explorationThe fully automatic reaction calorimeter is efficient, safe, simple, and fully functional. This instrument is an automated reaction calorimeter under laboratory conditions, which can be widely used in reaction process design, process optimization and scaling up, process safety assessment, and other fields such as fine chemicals, pharmaceuticals, and third-party safety assessments.

2.The fully automatic reaction calorimeter follows the following standards:

uGB 51283 Fire Protection Standard for Engineering Design of Fine Chemical Enterprises；

uGB/T 22232 Determination of Thermal Stability of Chemical Substances Differential Scanning Calorimetry；

uGB/T Thermal analysis test method for dynamic constants of thermally unstable substances in 17802；

uSN/T 3078.1 Guidelines for Evaluating the Thermal Stability of Chemicals - Accelerated Calorimetry Method；

uNY/T 3784 Pesticide Thermal Stability Testing Method - Absolute Thermal Method.

Technical Specifications

1.Calorimetry methods: heat flow method, power compensation method, reflux (optional)

temperature control

2.Oil bath temperature range:-80℃～250℃

power control

3.Control mode: isothermal, constant temperature, scanning

4.Temperature resolution:1.0mK

5.Temperature control precision:±0.1K

6.Silicone oil circulation speed:40L/min～80L/min

7.Voltage range:0～50VDC

8.mostHigh current:3.0A， Optional 4.0A

9.heatermosthigh-power:120W

Reaction kettle

10.Volume of atmospheric pressure glass reactor:1L

11.Work pressure: Atmospheric pressure

12.Temperature range:-25℃～200℃

13.Atmospheric pressure reactor material: High quality3.3 Borosilicate Glass

14.Volume of high-pressure metal reactor:1L

15.work pressure10MPa

16.Temperature range:-55℃～200℃

17.High pressure reactor material:316L stainless steel

blender

18.mostHigh speed:50r/min-2000r/min

19.mostHigh torque:80N·cm， Optional 300N · cm

20.Mixing blade form: anchor or paddle type

21.Mixing blade material:316L

injection system

22.Injection channel:1 liquid injection, 1 solid injection port, expandable injection

23.Precision balance: range3100g， Precision 0.01g

24.Sample pump: electromagnetic diaphragm pump,mosthigh traffic2L/h

Basic Parameters

25.Power Supply:3*220V/50Hz（±10%）/20A

26.Power:7.2kw

27.Test area size:1360mm*680mm*1550mm

28.Oil bath size:610mm*108mm*1250mm

29.Oil bath weight:210kg

30.Total weight of the machine330kg

Features

1.There are three calorimeter methods available, including heat flow, power compensation, and reflux, which users can choose according to their needs；

2.Supports multiple operating modes such as isothermal, constant temperature, and scanning；

3.Simultaneously equipped with glass atmospheric pressure reactor and metal high-pressure reactor；

4.High power heating and cooling unit, fast temperature control response speed, high heat release measurement accuracy；

5.Automatic feeding control, which can achieve uniform mixing of substances in the mixing unit through mass or volume measurement；

6.Accurately measure and obtain reaction heat flux, reaction enthalpy, conversion rate, sample specific heat capacity, adiabatic temperature rise, and the achievable values of uncontrolled systemsmostProcess safety related data such as high temperature；

7.The operating software platform allows for flexible programming of experimental procedures, real-time monitoring of key data during the reaction process, and online modification of experimental procedures and required parameters；

8.Real time display of the temperature inside the kettle, jacket temperature, feeding quality, pressure, and other real-time test status；

9.Key parameters and state safety thresholds can be set, in case of reaction loss of controlOne click rapid cooling, abnormal state alarm and automatic shutdown, effectively ensuring safety；

10.Automatically generate and save charts and data, export experimental analysis reports；

11.USB interface plug and play, convenient for data management;

12.Red one button emergency stop button, which can directly cut off power in case of accidents, ensuring the safety of test personnel;

13.Instrument configuration15.6-inch capacitive touch screen, pre installed with professional operating software.

If you want to learn more about pricing, models, parameters, or have customized needs, please feel free to call or leave a message for consultation.