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E-mail
sales@kinochina.com
- Phone
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Address
D1-3F, No. 128 Shenfu Road, Xinzhuang Industrial Park, Minhang District, Shanghai
Corona Industries Inc. (Strategic Partner: Shanghai Solon Information Technology Co., Ltd.)
sales@kinochina.com
D1-3F, No. 128 Shenfu Road, Xinzhuang Industrial Park, Minhang District, Shanghai
Water droplet angle refers to the contact angle formed by water droplets on a solid surface, defined by the tangent angle between the gas-liquid and solid-liquid interfaces, and is a core parameter for evaluating surface cleanliness.Cleanliness measuring instrumentThrough high-precision droplet angle analysis (based on ADSA RealDrop) ® The Young Laplace equation fitting method of the algorithm quantifies the residual surface pollutants and energy state distribution, providing a basis for cleanliness grading for electronic components, optical glass, and other materials.
Specially designed for industrial scenarios, it integrates a manual liquid inlet system and a large stroke sample stage (compatible with 300mm wafers), equipped with an industrial grade telecentric lens and quartz soft light source, and supports multi area scanning of surface cleanliness such as PCB and touch screen. CAST ® The 2.0 software has a built-in dynamic contact angle tracking module that can synchronize dynamically changing contact angles (with an accuracy of ± 0.2 °) and liquid-liquid interface tension, meeting cleanliness detection standards.
Using precision optical mechanics and nanoscale titration technology (with a liquid control accuracy of 0.02 μ L), dynamic contact angle, surface free energy components (dispersion/polarity/hydrogen bonding force), and interfacial viscoelastic modulus were measured. The modular architecture supports the expansion of accessories such as high-pressure reaction tanks and vacuum environment chambers, and is suitable for harsh scenarios such as semiconductor pre packaging cleaning verification and medical implant biofilm detection.
| category | Application field | typical scenario | Cleanliness related indicators |
|---|---|---|---|
| basic research | Surfactant, lotion, polymer surface modification | Optimization of soap formula and evaluation of wetting properties of polymer coatings | Surface free energy component analysis (polarity/dispersion force ratio) |
| industrial manufacturing | Spray/paint/coating, paper/film/ink, aluminum foil hydrophilic angle test | Printing suitability testing, hydrophilic aluminum foil process validation | Contact angle hysteresis (<5 ° for high cleanliness surfaces) |
| Biomedicine | Wettability of artificial bone and interface characteristics of drug carriers | Compatibility testing of biomaterials and development of transdermal drug delivery systems | Protein adsorption inversion (contact angle>90 ° indicates low pollution) |
| Cleanliness testing and process control | PCB/chip/LCD surface cleanliness, plasma treatment effect, UV cleaning verification | Pre packaging cleaning evaluation of semiconductors and quality control of display panel coating | Water droplet angle ≤ 30 ° is considered to meet the standard (ASTM D5946) |
| Energy and Materials Science | Wettability of rock cores, hydrophobic coating of insulators, carbon fiber resin adhesion | Prediction of oil and gas extraction efficiency, optimization of composite material interface | Surface energy heterogeneity analysis (contact angle fluctuation>2 ° indicates contamination) |
| Standard code | Standard Name | Application scenarios for cleanliness detection |
|---|---|---|
| ASTM D 724 | Surface Wettability Test of Paper (Contact Angle Method) | Evaluation of Printing Suitability of Packaging Materials and Water Absorption Rate of Sanitary Products |
| ASTM D 5946-2004 | Measurement of water contact angle of polymer film treated with corona discharge | LCD screen polarizing film treatment effect, monitoring of surface energy of food packaging film |
| ISO 15989 | Measurement of water contact angle after corona treatment of plastic film | Validation of anti adhesion coatings for medical and catheter applications, optimization of industrial membrane material modification processes |
| test object | key parameters | judgment criteria | Instrument configuration requirements |
|---|---|---|---|
| Surface contaminants on wafers | Forward angle/backward angle difference | Δ θ<5 ° indicates A cleanliness | Nano level positioning platform (± 0.1 μ m), 1000x microscope lens |
| PCB pad oxide | Intrinsic contact angle (Young equation fitting) | θ<15 ° complies with IPC-A-610 | High temperature sample stage (200 ℃), nitrogen environment chamber |
| Medical implant biofilm | Surface free energy polarity component | Inhibition of bacterial adsorption by γ ^ P>35mJ/m ² | Biosafety grade sample warehouse, sterile injection system |
| Photovoltaic glass dustproof coating | roll angle | Alpha<10 ° has self-cleaning properties | Tilt table angle resolution 0.01 °, anti reflective light source |
——Integrated solution for precise interface chemical analysis and surface cleanliness evaluation
| module | Technical Characteristics | Cleanliness detection application |
|---|---|---|
| 10 dimensional ultra precision positioning | Cross linear guide rail technology (software control accuracy of 0.5 μ m)+aviation aluminum integrated fuselage, vibration suppression<0.1 μ m. | Support wafer/PCB multi-point scanning (10 × 10 grid) and visualization of surface pollutant distribution. |
| Intelligent droplet control | Nano level injection pump (precision 0.02 μ L), PTFE superhydrophobic needle, suitable for 5 μ L droplet transfer. | Accurately evaluate the surface energy changes after plasma cleaning, with a contact angle repeatability error of ≤ 0.5 ° (ASTM D5946). |
| Dynamic Rolling Angle Analysis | The overall rotating platform (resolution 0.0001 °) synchronously controls the movement of the lens and sample, with a center offset of<1 μ m. | Quantify the anti fouling performance of coatings (rolling angle<10 ° is considered a self-cleaning surface). |
| module | Technical Characteristics | Cleanliness detection application |
|---|---|---|
| Industrial grade optical system | 0.35-4.5X continuous zoom telephoto lens, distortion rate<0.08%+adjustable LED cold light source (470nm). | Identify 0.1 μ m particle pollutants and be compatible with wafer defect detection (1000x optional lens). |
| High speed dynamic capture | Original German 87fps camera (standard configuration), optional 300fps/1000fps high-speed module. | Record the process of droplet spreading/shrinking (25 frames per second) and analyze the dynamic characteristics of surfactant residue. |
| Environmental interference suppression | UV filter lens+shading film technology reduces background noise by 90%. | Stable measurement of the cleanliness of high reflective surfaces such as medical catheters and optical lenses in strong light environments. |
| functional module | Technical Characteristics | Cleanliness detection application |
|---|---|---|
| Multimodal Algorithm Library | 7 contact angle algorithms (including those based on ADSA RealDrop) ® The Young Laplace fitting method+12 surface free energy models. | Quantify pollutant types (organic/inorganic) through polar force components (γ ^ P), in compliance with ISO 15989 cleanliness classification standards. |
| Dynamic process analysis | Dual trigger technology synchronously collects contact angle/time curves and supports calculation of the viscoelastic modulus of oscillating droplets (E '/E' '). | Evaluate the adsorption kinetics of cleaning agents on chip surfaces and optimize CMP process parameters. |
| Cleanliness reporting system | One click generation of PDF report, including contact angle distribution heatmap, surface energy 3D mapping, and pollution risk assessment. | Compatible with the IPC-A-610 standard in the semiconductor industry, determining the degree of pad oxidation (θ>15 ° warning). |
| Database and Compliance | Preloaded with 800 liquid parameters, data can be exported in Excel/BMP format, in compliance with FDA 21 CFR Part 11 requirements. | Trace the cleanliness data of medical implant production batches to meet GMP audit requirements. |
| Application scenarios | detection parameters | Instrument configuration |
|---|---|---|
| Cleaning before semiconductor packaging | Water droplet angle (θ ≤ 30 ° meets the standard) | Temperature controlled sample stage (-20~200 ℃)+nitrogen purification chamber (optional) |
| Display screen polarizing film treatment | Forward/backward angle lag (Δ θ<5 °) | Surface correction module+anti reflection light source |
| Medical Device Biofilm Testing | Surface free energy polarity component (γ ^ P>35mJ/m ²) | Biosafety sample chamber+sterile injection system |
| Photovoltaic glass dustproof coating | Rolling angle (α<10 °) | Tilt table (0-90 °± 0.01 °)+100fps high-speed camera |
Technical Specifications
The following annotations“*”The main differences between each model are as follows.
| SL200L | SL200L+ | ||||||
| Instrument appearance diagram | |||||||
| Related model keywords | Standard contact angle measuring instrument /Interface tension meter | Large stroke contact angle measuring instrument /Interface tension meter | |||||
| Hardware configuration and specifications | Sample stage control | levelXmove | Manual travel:50mm Accuracy:0.1mm Upgradeable to maximum300mmitinerary | Automatic itinerary: 100mm*200mm Accuracy:0.01mm Upgradeable to maximum300mmitinerary | |||
| levelYmove | |||||||
| up and downZmove | Manual40mm Accuracy:0.01mm | manual 25mm Accuracy: 0.01mm
| |||||
| Sample table rotation | No, you need to purchase the SL200K series | ||||||
| level adjustment | Manually adjust the knob to control the level of the sample stage, the level of the entire machine, and the level of the lens | ||||||
| Sample stand | 50*50mm | 50*50mm | |||||
| Can hold the largest sample | 250(W)*∞(L)*50(H)mm | 250(W)*∞(L)*50(H)mm | |||||
| Other controls | syringeXYmove | trip:12.5mm Accuracy:0.01mm
| |||||
| Liquid inlet controlZ: Pipette transfer | Manual travel:12.5mm Accuracy:0.01mm
| Manual travel:12.5 Accuracy:0.01mm
| |||||
| Camera horizontal control | One dimensional pitch adjustment with locking function | ||||||
| Light shielding film technology | * Need to purchase separately | * Need to purchase separately | |||||
| accessories | Optional: Professional fiber clamps, professional film clamps, and plant leaf clamps can be used to analyze the contact angle values of fiber or surface uneven samples. | ||||||
| sampler | model | * Manual infusion pump | * Automatic infusion pump | ||||
| Standard precision | 0.01mm0.02uL | 0.02uLsyringe pump | |||||
| Transfer method | * Manual control of pipetting operation | * Automatic control of pipetting operation | |||||
| needle | Professional replaceable needle injection syringe, including0.5mmStandard needles0.9mmCoarse needle and contact angle value for testing superhydrophobic materials or adhesives on solid materials0.3mmStainless steel fine needle, PTFE needle, etc | ||||||
| imaging system | lens | Industrial continuous magnifying lens0.35-4.5XEffective pixels:35 -450 pixel/mm | |||||
| camera | 1Industrial grade black and whiteUSB2.0video camera; 2Resolution:752*480(Standard video)WVGAFormat); (Optional)130Ten thousand pixels300Ten thousand pixels500Ten megapixel or higher definition camera 3Image speed:87-340frame/Seconds; (Optional)100frame/In seconds300frame/In seconds1000frame/Second or higher) 4Standard format image conversion without image distortion; 5Communication interface:USB2.0No compatibility issues/optional1394Interface camera | ||||||
| light source system | Adjustable brightness monochrome cold lightLEDLight source, contact angle, clearer image edges | ||||||
| software system | Test droplet status, total5Species: Suspension Drop Method(Pendant Drop)Stop drip method(Sessile Drop)(2/3State), bubble capture method(Captive Drop)Insertion method, oscillation drop method(oscillating drop)Wait. | ||||||
| There are two types and seven or more methods for calculating contact angle: | |||||||
| Contact angle data acquisition method: a combination of fully automatic measurement and manual modification. Press' Test ', the software automatically completes taking photos-Find sensitive points-Calculate the contact angle value-Display the calculation results without manual intervention throughout the process to reduce the impact of human factors. | |||||||
| Contact angle measurement technology: combining mathematical model fitting with actual measurement of the actual droplet profile to solve the problem of asymmetric image measurement | |||||||
| Automatic surface correction: upward convex surface, downward concave surface, surface roughness correction; | |||||||
| move/Static contact angle test, capable of testing forward/Backward angle/Tilt angle and roll angle values | |||||||
| Image capture method: single or25frame/Continuous shooting at higher speeds requires the purchase of a corresponding speed camera, such as60Frame100Frame1000Camera with frame speed. | |||||||
| Dual software triggering technology can be used to obtain the contact angle at the first moment during the analysis of powders, paper, and other absorbent materials, as well as to capture the entire process of measuring small contact angles. | |||||||
| The function of calculating and comparing the left and right contact angle values separately, and the software automatically calculates the average contact angle | |||||||
| Automatically generate a curve graph that allows real-time observation of changes in contact angle | |||||||
| Database management function: one-to-one correspondence between data and images, backup, compression, and exportEXCELThe table, measurement values, and curve fitting results can all be saved to the exported image, which is intuitive and clear. | |||||||
| Video recording function: recordingAVIFormat film and television images, which can be used forPPTDocument production. | |||||||
| Up to12A surface free energy estimation model, including: Equation of State ( Neumann et al. )TheGood-GirifalcoTheOwen-Wendt-RabelTheSimple FowkesTheExtended FowkesTheWUlaw1-2TheSchultzlaw1-2TheAcid-base(Van OSS & Good)TheJhuTheZizmanCritical surface tension method, etc12A method for estimating surface free energy can be used to analyze not only low-energy solid surfaces, but also high-energy solid surfaces, as well as their distribution (dispersion force, polarity force, hydrogen bond value, Lewis acid-base, etc.) | |||||||
| Powerful wettability analysis function(Wetting Behavior Analysis WBA®Analysis) | |||||||
| Automatic droplet volume, adhesion work, and one liquid method surface free energy analysis function, which can be used to test the surface tension value of thin films and can replace the testing function of Dyne pens | |||||||
| Universal indicators | Scope of contact angle testing | 0°<θ<180° | |||||
| Reading resolution | 0.01° | ||||||
| test accuracy | ±1° (θ/2law)±0.1°Circle simulation is legal | ||||||
| Interface tension testing range | 0.001-2000mN/m | ||||||
| Resolution of interface tension test | 0.001mN/m | ||||||
| Interface tension testing method | BATable(select plane)TheYoung-LaplaceFitting Technology (Fourth Generation) | ||||||
| Host size and weight | 300Wx650Lx600Hmm 23-30kg | ||||||
| power supply | AC100~240V 50/60HZ | ||||||
Attachment:
1Temperature control device:
Including(1)Sample temperature control(2)Testing liquid temperature control;
These are two temperature control systems that respectively control the temperature of liquid and solid samples. It can be purchased separately or simultaneously.
→The temperature control method for solid samples can be selected from one of the following two temperature control methods:
(1)Thermostatic water bath control:0-95℃The temperature error is0.1℃;
(2)Semiconductor heating and cooling:5-85℃,Temperature error is0.5℃;
(3)Special temperature heating system: such as200℃The400℃The temperature control requirements can be confirmed with us.
→It is recommended to use a constant temperature water bath for liquid temperature control.
2High temperature contact angle test: maximum achievable1400、1700、1800、2000Degree contact angle test; Customized products require a deposit.
3Vacuum environment device: realizes contact angle testing under vacuum or different gas environments; Customized products require a deposit.
4Sample slot: effectively control the shaking of the sample and the influence of temperature, light, etc; Customized products require a deposit.
5High temperature interfacial tension test: The interfacial tension test between melted solid materials and air is conducted using hanging drop or stopping drop interfacial tension analysis techniques. Customized products require a deposit.
6Full range of needle tubes and needles
including:25uLThe100uLThe500uLThe1000uLHigh precision microsampler、And PTFE needles, stainless steel needles (various diameters), plastic needles, bent needles, etc
7High precision dual channel software controlled automatic injection pump
8Specialized fixtures: used for clamping fibers, films, paper, etc
9Quartz glass sample tank for bubble capture method
10Oscillatory droplets(oscillating drop)test module
(1)By using high-frequency oscillators and closed-loop oscillation control systems, the control accuracy is higher and the control method is more flexible. Oscillators with different oscillation frequencies and amplitudes can be selected according to customer needs.
| serial number | Oscillation amplitude | Maximum oscillation frequency |
| 1 | 2uL | 100z |
| 2 | 10uL | 100Hz |
| 3 | 10uL | 60Hz |
| 4 | 20uL | 60Hz |
(2)Optional injection needle tube:0.5uLThe1uLThe5uLThe15uLThe100uLThe500uLThe1000uLWait.
(3)Oscillatory waveforms include positive arc waves, residual arc waves, triangular waves, linear waves, sawtooth waves, etc., with a frequency of2KHzNo attenuation or distortion within.
CAST2.0Example of real image testing for image analysis system
1Analysis of Forward and Backward Angle: Real Image
image1 Analysis method: Curve ruler fitting method (circle fittingsplineFitting, generalized quadratic curve fitting, etc.
Forward angle/It is recommended to purchase injection pumps or peristaltic pumps for the setback angle test. Forward angle/There are two ways to form a setback angle:(1)Increase/Reduce droplet volume to form forward movement/Backward angle; (2)The sample table tilts to form a forward and backward angle. As shown in the figure above
2 Real graph of irregular contact angle analysis:
The picture shows the actual effect of silicone gel, and the contact angle value is calculated using curve ruler fitting technology. Fitting factor90%The above.
image2 Analysis method:SplineCurve fitting method orYoung-LaplaceEquation fitting method
Special statement:
1The above image information and technical parameters are subject to changes due to design without further notice, and the latest confirmed product information shall prevail.
2Our company reserves all rights.
3. Asha ®、 RealDrop ®、 TrueDrop ®、 MicroDrop ®、 WBA ®、 ADSA ® It is a registered trademark of Shanghai Solon.
CAST®Asha®、ADSA®、TrueDrop®、RealDrop®、TheDrop®、MicroDrop®、LMCA®、Shsolon®Solon®Register a trademark for Shanghai Solon.
The above trademark is used for goods or services related to contact angle measuring instruments, surface tension meters, and interfacial tension meters. Infringement will be prosecuted!