Microwave hydrothermal synthesis instrument

NegotiableUpdate on 02/03

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Nature of the Manufacturer: Producers

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Overview

The instrument adopts imported Toshiba brand professional microwave source, which is uniformly heated by microwave and heats up quickly. The chamber is made of large volume austenitic stainless steel material, and the inner cavity is imported with Teflon spray coating, with a thickness of five layers, and has the functions of high temperature resistance and corrosion resistance. It can simultaneously handle 6 ultra-high pressure and large capacity (100m) reaction vessels. Specially designed dual protection safety furnace door, multi-layer composite integrated mold stamping high-strength anti radiation leakage furnace door, with safety performance such as no deformation, shock wave resistance, and microwave leakage prevention. Temperature and pressure dual control system, with real-time display of reaction data on the LCD screen. Using safety explosion-proof film to prevent damage to the tank body and harm to the human body.

Product Details

Microwave system

Imported microwave source: Toshiba brand microwave source is used, with an input power of ≥ 1500W and an output power of ≥ 1000W. The continuous working time of the microwave source is ≥ 48 hours;
Microwave frequency: 2450MHz;
Microwave power: 0~1000W automatic continuous infinitely adjustable;
Continuous microwave power output, PID precise control algorithm, adaptively adjusts microwave power according to preset time to ensure smooth microwave power output.

Temperature control system

High precision contact PT1000 titanium alloy temperature sensor, greatly improving corrosion resistance;
[Range] Temperature measurement range: 0-300 ℃; Maximum operating temperature: 260 ℃;
[Accuracy] Temperature measurement accuracy: ± 0.1 ℃; Temperature control accuracy: ± 1 ℃; Display accuracy: 0.1 ℃;
Rate heating, programmed temperature control: reaching the target temperature at a uniform and precise speed within the set time;
[Over temperature protection] Real time monitoring of the temperature inside the digestion tank, which can automatically stop microwave emission when the temperature exceeds the set range and safety range, ensuring experimental safety;
【 Cooling and Cooling 】 Equipped with powerful and fast air cooling, using corrosion-resistant, high air volume centrifugal exhaust fans. After the reaction is complete, the microwave stops emitting, the fan continues to work, and the instrument displays the temperature and pressure values inside the reaction kettle in real time. When the digestion tank cools down, the instrument beeps to remind the end of the experiment.

Pressure control system

High precision contact pressure sensor, real-time detection of the true pressure inside the reaction vessel;
150-200 data/second;
Measurement range: 0-10MPa; The maximum working pressure is 6MPa; Measurement accuracy: 0.01MPa; Control pressure accuracy ± 0.05MPa;

After sales cooperation

【 One year warranty 】 The instrument comes with a one-year overall warranty, excluding consumables and accessories;

Lifetime maintenance: After the warranty period expires, lifetime maintenance will be provided, and only the cost of replacing parts will be charged. No other fees such as on-site fees will be charged;

【 Research Support 】 Upon receiving inquiries from users regarding the possibility of experiments, instrument operation, and troubleshooting, professional technicians will respond within 2 hours. If the fault is reported for repair, it can arrive at the scene within 48 hours!

Furnace cavity system

Microwave resonant cavity made of austenitic stainless steel, with multi-layer Teflon coating for strong acid corrosion resistance;
【 Door Protection 】 Specially designed dual protection safety furnace door, multi-layer composite integrated mold stamping high-strength anti radiation leakage furnace door, with safety performance such as no deformation, shock wave resistance, and microwave leakage prevention;

High pressure reaction unit

【 Detachable digestion turntable 】 Place 6 microwave high-pressure reaction vessels on the rotating turntable, and rotate the turntable uniformly 360 ° in one direction to ensure uniform microwave irradiation on each microwave high-pressure reaction vessel, improving the consistency of parallel experiments;
The outer tank of the high-pressure reaction vessel is made of imported modified polyetheretherketone resin composite material, and the inner tank is made of modified polytetrafluoroethylene; The maximum working temperature is 260 ℃; The maximum working pressure is 6MPa (870psi).

Instrument control system

[Program Temperature Control] Set reaction parameters in sections, totaling 10 sections. Each working section can set microwave power, temperature, and time according to experimental needs, and can store 16 sets of set parameters;
Rate heating, reaching the target temperature at a constant speed within a preset time, programmed temperature control;
During the experiment, the screen can display the temperature, time, power, pressure values, and curve of the reaction system in real time;
Remote control: Stop responding remotely in emergency situations;

Security protection system

[Chamber door protection] Dual safety door lock, automatically cuts off microwave power protection when the chamber door is opened;
【 Pressure relief protection 】 Safety explosion-proof membrane is used. In case of accidental overpressure, gas will rush out from the pressure relief hole to ensure experimental safety;

Quality Certification

Guojiaji's research achievements in industry university research innovation

【 ISO9001 Product Quality System Certification 】 The instrument has passed ISO quality certification, with high performance and high quality;

Compliant with national security standards