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Shanghai Yiji Industrial Co., Ltd
5972 Zhangyang North Road, Pudong New Area, Shanghai
2-Sulfonylbenzoic anhydride81-08-3 99% g/kg standard reference substance
Chinese name2-Sulfonylbenzoic anhydrideChinese synonym for sulfonamide; 3H-2, 1-Benzothiol-3-one-1,1-dioxide; Ortho sulfobenzoic anhydride; 2-Thiobenzoic anhydride; 2-Sulfonic acid benzoic anhydride; Sulfonylbenzoyl anhydride; 2-Thiobenzoic anhydride, 94%; 2,1-Benzothiol-3-one-1,1-dioxide
Point 116-124 ° C Boiling point 184-186 ° C18mmHg (lit.) Density 1.6114 (roughness) Refractive index 1.6290 (estimate) Flash point 184-186 ° C/18mm Storage conditions Storebelt+30 ° C. Solubility in toluene form crystals or crystalline powders Color white to beige Sensitivity Overview 2-sulfobenzoic anhydride is an acid anhydride derivative that can be used in the pharmaceutical and chemical industries. The application examples of 2-sulfobenzoic anhydride are as follows: 1. Preparation of flame retardant and light resistant waterborne polyurethane coatings; 2. Preparation of a carbon nanotube graphene modified waterborne polyurethane coating and adhesive. The preparation of 2-sulfobenzoic anhydride is as follows: Under N2 protection, 9.0g of saccharin solid and 13mL of concentrated sulfuric acid (concentration 98%) are sequentially added to a 50mL three necked flask, stirred at 140 ℃ for 2 hours, cooled to room temperature, and a large amount of solid is precipitated in the reaction mixture. The filtered solid is washed with ice water and dried to obtain 7.3g of white 2-sulfobenzoic anhydride with a yield of 81%.
2-Sulfonylbenzoic anhydride81-08-3 99% g/kg standard reference substance