Microwave chemical synthesis extractorIt is a laboratory equipment that combines microwave heating and chemical synthesis/extraction technology. Its core advantage lies in an efficient, uniform, and controllable heating method, which can significantly shorten reaction time, improve yield, and reduce by-product generation.
Microwave chemical synthesis extractorUsage method:
1. Sample preparation:
Choose polar solvents or reaction systems containing ions;
The sample volume should not exceed 2/3 of the container volume (to prevent boiling overflow), and a pressure buffer space should be reserved for closed reactions;
Avoid using metal containers and recommend polytetrafluoroethylene (PTFE), quartz, or high borosilicate glass containers.
2. Parameter settings: Set the microwave power (50% -80% to avoid local overheating caused by full power), target temperature, reaction time, and enable stirring and temperature/pressure monitoring according to experimental requirements.
3. Experimental process: Real time observation of equipment operation status. If there is a "chamber ignition" or "sudden pressure rise", immediately pause and release the pressure; After the reaction is complete, wait for the sample to cool to room temperature before removing it (to prevent burns or solvent boiling).
4. Post treatment: Clean the chamber (wipe the inner wall with ethanol to remove residual samples), clean the container, turn off the power and cooling system.
The core advantages of this device lie in precise temperature control, high efficiency and energy saving, and shortened experimental cycles. It is widely used in fields such as organic synthesis, drug research and development, food testing, and environmental sample pretreatment, and is one of the key equipment for improving efficiency in modern chemical laboratories.