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What are the advantages of reactive distillation in the experimental process
Date: 2025-05-20Read: 1

Distillation is a typical unit operation for separating miscible liquid mixtures in chemical production. Its essence is multi-stage distillation, which uses the different boiling points or saturated vapor pressures of each component in the miscible liquid mixture under a certain pressure to vaporize light components (components with lower boiling points or higher saturated vapor pressures). After multiple partial liquid-phase vaporization and partial gas-phase condensation, the concentration of light components in the gas phase and heavy components in the liquid phase gradually increases, thereby achieving separation. The raw materials are fed into the tower from an appropriate position in the middle, and the tower is divided into two sections. The upper section is the distillation section, which does not contain feed, and the lower section, which contains a feed plate, is the retention section. The condenser provides liquid-phase reflux from the top of the tower, and the reboiler provides gas-phase reflux from the bottom of the tower. Gas and liquid reflux are important characteristics of distillation.

Usage characteristics:
1. Experimental scale solvent distillation recovery.
2. Steel frame, beautiful appearance, strong corrosion resistance.
3. High borosilicate glass kettle body, with strong corrosion resistance, suitable for various occasions. Intuitive and intuitive reaction process, easy to observe phenomena.
4. The horizontal three-layer serpentine tube condenser has a large condensation area and high efficiency.
5. The types of materials that can be used to fill the distillation column are widely applicable.
6. By utilizing the characteristics of its double-layer glass, the reaction material (some called reaction solvent) can be placed in the middle interlayer and stirred under normal pressure or negative pressure. The glass reaction kettle is filled with a constant temperature (high or low temperature) hot solution or coolant through the double-layer reaction kettle interlayer, and the materials in the reaction kettle are heated or cooled at a constant temperature, and can also be stirred.
Reactive distillation interlayerDifferent cold and hot circulation liquids (hot water/hot oil/frozen liquid) can be introduced, and the reactants can be stirred and reacted under normal pressure or negative pressure in a sealed glass bottle. The fully transparent reaction process is clear at a glance, making it an ideal pilot test equipment for modern biopharmaceuticals, fine chemicals, and new material synthesis.