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Shanghai Chromatography Instrument Co., Ltd
Rohs2.0 detection gas chromatography-mass spectrometry system
NegotiableUpdate on 07/07
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Overview
Rohs2.0 detection gas chromatography-mass spectrometry system - Method summary - Referring to GB/T 29786-2013 Determination of Phthalates in Electronic and Electrical Products - Gas chromatography-mass spectrometry method, use gas chromatography-mass spectrometry to detect mixed standards of phthalates. Qualify the phthalate standard based on retention time, mass spectrum, and characteristic ions, and determine the external standard quantity.
Product Details
Rohs2.0 detection gas chromatography-mass spectrometry system
serial number |
name |
quantity |
1.1 |
Mass spectrometer: |
1 set |
1.1.1 |
Single quadrupole mass spectrometer host |
1 |
1.1.2 |
250 L/s molecular turbo pump |
1 |
1.1.3 |
Front stage vacuum pump 4m3/h |
1 |
1.1.4 |
Gas chromatography-mass spectrometry transmission line |
1 |
1.1.5 |
Inert EI ion source |
1 |
1.2 |
Gas chromatograph: |
1 set |
1.2.1 |
Gas chromatograph host, pressure control accuracy 0.001psi |
1 |
1.2.2 |
Split/No Split Injection Port, with EPC |
1 |
1.3 |
Workstation software: |
1 set |
1.3.1 |
Qualitative and quantitative analysis software for gas chromatography-mass spectrometry V1.0 |
1 |
1.4 |
Spare parts and consumables: |
1 set |
1.4.1 |
Gas Chromatography Startup Kit |
1 |
1.4.2 |
Temperament test standard sample |
1 |
1.4.3 |
Mass spectrometry maintenance toolkit |
1 |
1.4.4 |
Mechanical pump oil 1L |
1 |
1.4.5 |
Pushing ceramic pads, 10 per pack |
1 |
1.4.6 |
Gloves, double |
5 |
1.4.7 |
Dust free cloth, block |
5 |
1.4.8 |
Cotton swab, bag |
1 |
1.4.9 |
Ion source polishing powder, bottle |
1 |
1.4.10 |
MS interface column nut, internal thread |
1 |
1.4.11 |
HP-5HT 15m*0.25mm*0.25um |
1 |
1.4.12 |
Helium trap |
1 |
1.4.13 |
24 bit liquid automatic sampler |
1 |
1.5 |
computer |
1 set |
1.5.1 |
computer:Win10 dual core 4G or above memory 64 bit system |
1 |
1.5.2 |
Printer: Color |
1 |
1.5.3 |
UPS power supply: 6KW |
1 |
1.6 |
Reagentsreference standardAnd gas source |
1 set |
1.6.1 |
*Chromatographic purity, 4L/bottle |
1 |
1.6.2 |
phthalene4P MixStandard product:BBP、DIBP、DBP、DEHP |
1 |
1.6.3 |
Polybrominated biphenyl standard solution, polybrominated diphenyl ether standard solution |
1 |
1.6.4 |
helium，Purity 99.999%，40L/bottle,Equipped with pressure reducing valve |
1 |
Method SummaryReferring to GB/T 29786-2013 Determination of Phthalates in Electronic and Electrical Products by Gas Chromatography Mass Spectrometry, a gas chromatography-mass spectrometer is used to detect mixed standards of phthalates. The phthalate standard is qualitatively determined based on retention time, mass spectrum, and characteristic ions, and the external standard is used to determine the amount.
test method
Injection mode: pulse non split injection; Pulse pressure: 20psi; Pulse time: 0.75min; Blow flow rate of 60ml/min; Purging time: 1 minute;
Injection volume: 1 μ L;
Column: DB-5HT, 15m × 0.25mm × 0.1 μ m Column Flow Rate: 1ml/min
Column box heating program: 60 ℃ (1 minute) 10 ℃/min 180 ℃ 5 ℃/min 250 ℃
Injection port: 280 ℃; Ion source: 300 ℃; Transmission line: 280 ℃;
Solvent delay: 8 minutes;
Scanning mode: Full Scan (SCAN) or Selective Ion (SIM); Scanning range: 50~500 amu.
Test chart
Full scan total ion chromatogram
10 types of phthalates 10mg/L full scan total ion chromatogram
1,DIBP； 2，DBP； 3，DPP； 4，BBP； 5，DNHP； 6,DCHP； 7,DEHP； 8,DNOP； 9,DINP； 10,DIDP
Method SummaryReferring to GB/T 26125-2011 Determination of six restricted substances (lead, mercury, cadmium, hexavalent chromium, polybrominated biphenyls, and polybrominated diphenyl ethers) in electronic and electrical products, 17 polybrominated biphenyls and polybrominated diphenyl ether mixed standards were detected using gas chromatography-mass spectrometry. The polybrominated biphenyl standards were qualitatively determined based on retention time, mass spectra, and characteristic ions, and quantified using external standard method.
test method
Injection mode: pulse non split injection; Pulse pressure: 20psi; Pulse time: 0.75min; Blow flow rate of 60ml/min; Purging time: 1 minute;
Injection volume: 1 μ L;
Column: DB-5HT, 15m × 0.25mm × 0.1 μ m Column Flow Rate: 3ml/min
Column box heating program: 100 ℃ (1min), 30 ℃/min, 340 ℃ (4min)
Injection port: 280 ℃; Ion source: 350 ℃; Transmission line: 340 ℃;
Solvent delay: 2.5 minutes; Multiplier voltage: tuning voltage of 0.2KV;
Scanning mode: Full Scan (SCAN) or Selective Ion (SIM); Scanning range: 100~1000 amu.
Test chart
Full scan total ion chromatogram
17 kinds of polybrominated biphenyls and polybrominated diphenyl ethers mixed standard 5mg/L full scan total ion chromatogram
1. Monobromobiphenyl; 2. Monobromodiphenyl ether; 3. Dibromobiphenyl; 4. Dibromodiphenyl ether; 5. Tribromobiphenyl; 6. Tribromodiphenyl ether; 7. Tetrabromobiphenyl; 8. Pentabromobiphenyl; 9. Tetrabromodiphenyl ether; 10. Hexabromobiphenyl; 11. Pentabromodiphenyl ether; 12. Hexabromodiphenyl ether; 13, heptabromodiphenyl ether; 14. Octabromodiphenyl ether; 15. Pentabromodiphenyl ether; 16. Decabromobiphenyl; 17. Decabromodiphenyl ether
Rohs2.0 detection gas chromatography-mass spectrometry system
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