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Shanghai Xinyi Microwave Chemical Technology Co., Ltd
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High throughput closed microwave digestion/extraction/synthesis workstation

NegotiableUpdate on 12/19
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Overview
The MASTER series high-throughput closed microwave digestion/extraction/synthesis workstation was born in 2012 and is a representative of Shanghai's new instrument technology and manufacturing process. The MASTER series can be adapted to 16 tank independent frame high-pressure digestion rotors, 18 tank rotary table integrated ultra-high pressure digestion rotors, 40/100 tank rotary table integrated medium high pressure digestion rotors, 14 position 200ml rotary table integrated ultra large capacity rotors, etc., to meet different laboratory application needs. Other core technologies of MASTER include: materials and processing technology for aerospace fiber Xtra Fiber digestion outer tank, quantitative safety release tablet Safet
Product Details

MASTER seriesHigh throughput closed microwave digestion/extraction/synthesis workstationIt is a typical representative of Shanghai Xinyi microwave products, which effectively combines high-throughput and ultra-high voltage technology. The MASTER series can be adapted to various specifications of digestion tank rotors to meet the application needs of different users.


Product comprehensive technical characteristics


safety



Comprehensive temperature and pressure measurement and control technology ensures safe and controllable operation process, effectively responding to any abnormalities

Temperature measurement and control: The direct measurement and control of the main control tank temperature is combined with infrared full tank scanning temperature control technology. The instrument automatically recognizes the real-time temperature comparison between the main control tank and the standard tank, which has higher accuracy and more reliable control than using infrared temperature measurement alone.


Pressure measurement and control: Shanghai Xinyi adopts piezoelectric crystal pressure measurement technology, which has reliable performance, no cross contamination, and a pressure control range of 0-15MPa (about 2200psi). The measurement and control cable will not be twisted or broken, there is no sealed interface, there will be no air leakage, and the operation is simple.



Safe release tabletSafety BoltDesign, fully enclosed digestion while achieving quantitative and safe pressure relief

Based on nearly 30 years of industry experience, Shanghai Xinyi adopts a safety relief plate structure design to ensure that the digestion tank is in normal working condition

Sealed and leak free, the pressure relief plate automatically lifts to release pressure under overpressure, ensuring safe operation. Under normal operating conditions, the safety relief tablet will not rupture and does not require replacement, there are no consumables, and there is no risk of leakage.



High strength aerospace composite fiber outer tank, balancing mechanical strength and anti-corrosion ability

High strength aerospace composite fiber outer tank Xtra Fiber, PFA overall spraying wraps the composite fiber, which has the characteristics of being unbreakable, unbreakable and tear resistant. Its comprehensive performance in pressure resistance, corrosion resistance and other aspects is superior to traditional PEEK material outer tanks (especially the protective ability at the edge of the outer tank). The compressive strength can reach 70MPa (about 10000psi), and the temperature resistance is 600 ℃, ensuring the safety of the user's operation.



The high-strength alloy rotor is under overall pressure, ensuring that the tank body does not deform or leak under long-term pressure

The high-throughput tank rack is connected as a whole with high-strength alloy material pull rods, providing strong pressure support. The top and bottom of each digestion tank can be supported vertically by the rack, ensuring that the digestion tank does not deform or leak during high-temperature and high-pressure digestion.



Auto-PopSafe explosion-proof sliding furnace door design ensures the personal safety of operators

Pop up buffer safety explosion-proof sliding furnace door, making operation more reassuring and safe. The furnace door dual locking self checking system has a dual electronic and mechanical design, making it easy to operate.


efficient



Multiple flux digestion tank rotor combinations to meet different application requirements

The MASTER series can accommodate 16 independent frame high-pressure digestion rotors or 40 high-throughput digestion rotors for conventional needs; For certain customers' special application requirements, such as 18 tank combined ultra-high pressure rotors, they can also be met. The instrument has good scalability and high sample compatibility, which helps researchers improve work efficiency.



Digestion ability to meet the digestion needs of special samples

2200W high microwave output power, frequency conversion non pulse continuous microwave emission, and dual magnetron two-dimensional bidirectional arrangement, the microwave field is more uniform, the energy utilization rate is higher, and it meets the digestion needs of special samples.



High throughput tank rackUTH-CaroDesign to stir the microwave magnetic field evenly during rotation, ensuring uniform digestion of high-throughput samples

The UTH Caro high-throughput tank rack is designed with metal components that allow the microwave field inside the furnace to stir with the rotation of the rack. Even 100 high-throughput digestion tanks can ensure heating in a uniformly distributed microwave field, ensuring uniform and consistent digestion effects.



The fully enclosed high-pressure digestion technology effectively improves the recovery rate and ensures the accuracy of data results

By using a high-pressure digestion tank, the digestion capacity is improved, and the advantages are obvious for difficult to digest samples and samples that are prone to high pressure. The fully enclosed high-pressure digestion mode does not release pressure throughout the entire digestion process, especially for elements that are prone to volatile loss, and the recovery rate is satisfactory.


reliable



Durable and sturdy industrial grade furnace chamber, with comprehensive anti-corrosion coating inside and outside the furnace chamber to extend its service life

The sturdy and corrosion-resistant 316L stainless steel furnace chamber has a wall thickness of over 3mm, which can effectively absorb impacts in special situations and protect personnel safety. The inner and outer double-sided multi-layer PFA spray coating prevents corrosion of the furnace chamber by acid mist, extends the service life of the furnace chamber, and has a 5-year warranty commitment.



Uni-TurnSynchronized rotation technology to improve instrument reliability

By adopting Uni Turn technology, the upper temperature and pressure sensor and rotor can rotate synchronously, ensuring high-precision temperature and pressure measurement while avoiding sensor entanglement, effectively reducing motor load, and improving instrument reliability.


High power and efficient exhaust system to prevent internal corrosion of equipment

Adopting a high-power fan design, it can timely discharge acid mist, avoid internal corrosion of equipment, and effectively cool the furnace cavity during digestion, avoiding a decrease in mechanical performance of pressure bearing components.


convenient



Various supporting operation tools make digestion work easy and simple

A mobile and flexible tool cart can help experimenters easily place or remove high-throughput turntables filled with samples into or out of the furnace chamber. The fixed torque electric tool makes the sealing and opening operation of the digestion tank easy and simple.


Rich application methods can be easily managed and accessed, making digestion experiments convenient and efficient

The instrument is equipped with a rich and safety validated digestion method library, covering over 1000 types of samples and compatible with standard methods such as US-EPA and ASTM. Users can also edit and store their own method library as needed. The high-definition LED display screen can display experimental parameters and curve changes in real time, with a user-friendly interface and easy operation.


‍‍ ‍microwave digestion/extraction/Synthesize different module combinations to meet different application needs, convenient and flexible‍

MASTERThe series of microwave chemistry workstations can easily complete high-pressure and high-throughput digestion experiments, flexibly replace different reagents and tanks, and perform microwave extraction and synthesis work. One machine is versatile, fully utilizing the characteristics and advantages of microwaves, providing more convenience and possibilities for technology workers and engineers in various industries.‍‍



Wireless remote visual monitoring system, making the internal operation status of the furnace chamber clear at a glance

Equipped with a remote visual monitoring system, the digestion process is well understood. Remote observation and monitoring of the digestion process can be achieved by using a mobile phone or tablet, further enhancing the operational experience.


Host technical parameters:

power supply

220~240VAC 50/60Hz 16A

Microwave source

2450MHz, Variable frequency dual magnetron high-energy microwave field emission

Installation power of the whole machine

3600W

Maximum output power of microwave

2200W

Microwave oven cavity

65L large volume 316L stainless steel chamber, with multiple layers of corrosion-resistant PFA spray coating inside and outside

Design of safety explosion-proof door

Six story steel structure self ejecting safety explosion-proof sliding furnace door, electronic/mechanical dual control

Pressure measurement system

Piezoelectric crystal sensor, voltage control range: 0~15MPa (about 2200psi), control accuracy ± 0.01MPa

Temperature measurement and control system

High precision platinum resistance temperature sensor+full tank infrared dual temperature measurement, temperature control range: 0~350 ℃, temperature control accuracy: ± 0.1 ℃

Passive protection system

Adopting a top safety bolt design, overpressure directional and quantitative release

Communication interface (optional)

USB,RS232

Video surveillance (optional)

Optional internal camera for real-time wireless monitoring of the operation of the digestion tank inside the furnace cavity

Furnace cavity exhaust system

Cooling to room temperature for less than 15 minutes

Working environment temperature/humidity

0~40℃ / 15~80%RH

Physical dimensions/net weight of the entire machine

580 × 690 × 700 (width x depth x height)/72kg


Supporting various flux digestion tanks and rotor specifications:

Name of reaction tank

16 position high-pressure tank

18 position ultra-high pressure tank

40 position medium and high pressure tank

Reaction tank model

GP-100

XXP-100

HP-40

Batch processing volume

16

18

40

Inner tank material

TFM

TFM

TFM

Outer tank material

Aerospace composite fiber

Aerospace composite fiber

Aerospace composite fiber

Rotor frame structure

Independent framework

Alloy turntable integrated frame

Alloy turntable integrated frame

Reaction tank capacity

100

100

70

design temperature

310

320

300

design pressure

15MPa (approximately 2200psi)

18MPa (approximately 2600psi)

10MPa (approximately 1450psi)

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