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E-mail
2084143512@qq.com
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Phone
18117403825
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Address
Haier Zhigu, Guangfulin East Road, Songjiang District, Shanghai
Shanghai Baosheng Industrial Development Co., Ltd
2084143512@qq.com
18117403825
Haier Zhigu, Guangfulin East Road, Songjiang District, Shanghai
Principles and processes
1. gas chromatography(GC)
Separate volatile compounds from the sample.
By chromatography column and carrier gas(Like helium gas)Implement separation.
2. smell test(Olfactometry)
The compounds separated by chromatography are passed through a splitter, with a portion entering the mass spectrometer and another portion entering the sniffing port.
The sensory evaluator sniffes the odor through their mouth and records the characteristics and intensity of the odor.
3. mass spectrometry(MS)
Identify the separated compounds and provide molecular weight and structural information
instrument composition
1. gas chromatograph
Chromatography column: commonly used capillary column(asDB5).
Injection system: liquid or headspace injection.
2. shunt
Divide the effluent into two parts and enter the mass spectrometer and sniffing port respectively.
3. Sniffing port
Equipped with a humidification device to prevent sensory evaluators from experiencing dry nasal passages.
4. mass spectrometer
Common electron bombardment ion sources(EI)And quadrupole mass analyzer.
sample pretreatment
1. Extract volatile compounds
Headspace injection(HS)Suitable for high volatility compounds.
Solid-phase microextraction(SPME)Adsorption of volatile substances through fibers.
Solvent extraction: using organic solvents(Like dichloromethane)Extract.
2. Concentration and Purification
Concentrate low concentration samples(Like nitrogen blowing).
Remove interfering substances(Such as fat and protein)