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Weihai Borui Chemical Machinery Co., Ltd

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    Yangting Beiguan Industrial Park, Huancui District, Weihai City, Shandong Province

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500l high-pressure hydrogenation kettle

NegotiableUpdate on 05/06
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Overview

The 500l high-pressure hydrogenation kettle is suitable for large-scale and continuous production and has important industrial applications. For example, acetylene and propyne in petroleum cracking gas can be partially hydrogenated by palladium catalysis to produce high-purity ethylene and propylene. In the oil and fat industry, liquid oil is hydrogenated into solid or semi-solid fat to produce hardened oil for artificial butter or soap industry.

Product Details

500l high-pressure hydrogenation kettleIntroduction:

The key to catalytic hydrogenation is the catalyst. They can be roughly divided into two categories:

1. Low pressure hydrogenation catalysts mainly consist of highly active Raney nickel, platinum, palladium, and rhodium. Low pressure hydrogenation can be carried out at 1-4 atmospheres and lower temperatures;

2. High pressure hydrogenation catalysts are mainly active materials such as Raney nickel and cuprous chromate. High pressure hydrogenation is usually carried out at temperatures between 100 and 300 atmospheres. Nickel catalysts are widely used, including various types such as Raney nickel and nickel boride. The characteristic of precious metal platinum and palladium catalysts is high catalytic activity, and their dosage can be much less than nickel catalysts. When platinum is used as a catalyst, most of the ene bonds can be reduced under conditions below 100 ℃ and atmospheric pressure.

Most industries use platinum and palladium as carriers, and those using activated carbon as carriers are called platinum carbon and palladium carbon, respectively. Copper chromite Cu (CrO2) 2 has a low cost and is widely used in industry. Its characteristic is that it is particularly effective in catalyzing carbonyl groups, and has high catalytic ability for ester groups, amides, imides, etc. It has low activity for alkene and alkyne bonds, and is basically inactive for aromatic rings.



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500l high-pressure hydrogenation kettlePurpose:;

Catalytic hydrogenation is suitable for large-scale and continuous production and has important industrial applications. For example, acetylene and propyne in petroleum cracking gas can be partially hydrogenated by palladium catalysis to produce high-purity ethylene and propylene. In the oil and fat industry, liquid oil is hydrogenated into solid or semi-solid fat to produce hardened oil for artificial butter or soap industry.

Palladium carbon is dissolved in ethanol and vacuum drawn into a high-pressure reactor or poured into the reactor. Then, ethanol is added to wash the container before being put into the reactor. After the reaction is complete, the material is filtered to recover palladium carbon. The reactor can be washed with reaction solvent and palladium carbon can be recovered through the filter.



(Hydrogenation reactor)500 liters

serial number

type

specific parameters

1

model

BR-500

2

Cauldron body

part

(1)volume

500 liters, open type, top flat cover and bottom head;



(2)pressure


Inside the kettle

jacket

Inner coil tube




Work pressure(MPa)

-0.1 ~ 0.5

0.6

0.4




Design pressure(MPa)

-0.1 ~ 5.0

0.8

0.6




Maximum allowable(MPa)

5.5

/

/



(3) Temperature


Inside the kettle

jacket

Inner coil tube




Working temperature(℃)

-10 ~ 50

-10 ~ 50

-10 ~ 50




Design temperature(℃)

-30 ~ 150

-30 ~ 150

-30 ~ 150



(4) Size


Inside the kettle

jacket

Inner coil tube




Inner diameter(mm)

800

950

Φ32




Straight edge height(mm)

950

950

/

thickness



Thickness(mm)

3+20

8

/



(5) Materials


Inside the kettle

jacket

Boiler coil inside the kettle




working medium

Methanol, isopropanol, hydrogen

steam

cooling water




medium characteristics

Moderate hazard, explosive

Non toxic, non flammable

Non toxic, non flammable




Liquid receiving components

S31603+16MnDR

16MnDR

S31603



(6) Processing

Internal surface polishing treatmentRa≤0.4μm, External surface painting;

3

stir

system

(1) Sealing

Magnetic coupling seal, zero leakage



(2) Rotational speed

motor

YB7.5KwExplosion proof grade DIICT4, explosion-proof variable frequency motor




speed reducer

TRXF88-YVB5.5-4P-3.78-M4, rotational speed300 revolutions per minute



(3) Paddle mixing

Efficient self-priming (propulsion)+Self suction+disc turbine

4

equipment

open one's mouth

Upper discharge port

DN32

With plug-in bottom tube



Solid feeding port

DN65

With blind plate



rupture disc/Pressure gauge port

DN40/15

Explosive fragments/Equipped with pressure gauge (digital display integrated, on-site display+remote transmission, range -0.1~1.0mpa, explosion-proof)



Vacuum exhaust port/Pressure gauge port

DN25/15

Equipped with pressure gaugeIntegrated digital display, on-site display+remote transmission, range -0.1~1.0mpa, explosion-proof,accuracy class±0.1℃)



hydrogen import

DN15

Equipped with bottom inserted hydrogen distributor



Liquid feed inlet

DN25




Temperature measuring port inside the kettle

M27*2

Equipped with platinum resistance for temperature measurement (on-site display)+Remote transmission, explosion-proof level CT4)



Lower the clean mouth

DN50

With blind blocking



Coil inlet

DN20




Coil outlet

DN20




Imported jacket

DN40




Jacket outlet

DN40




Jacket temperature measuring port

M27*2

Equipped with platinum resistance for temperature measurement (on-site display)+Remote transmission, explosion-proof level CT4)



Jacket exhaust port

M27*2

With blind blocking



(The opening of the equipment shall be subject to the final signed and confirmed drawings by both parties.)

5

other

Other unconfirmed matters shall be subject to the signed and confirmed drawings by both parties.