- Phone
-
Address
Yangting Beiguan Industrial Park, Huancui District, Weihai City, Shandong Province
Weihai Borui Chemical Machinery Co., Ltd
Yangting Beiguan Industrial Park, Huancui District, Weihai City, Shandong Province
500l high-pressure hydrogenation kettleIntroduction:
The key to catalytic hydrogenation is the catalyst. They can be roughly divided into two categories:
1. Low pressure hydrogenation catalysts mainly consist of highly active Raney nickel, platinum, palladium, and rhodium. Low pressure hydrogenation can be carried out at 1-4 atmospheres and lower temperatures;
2. High pressure hydrogenation catalysts are mainly active materials such as Raney nickel and cuprous chromate. High pressure hydrogenation is usually carried out at temperatures between 100 and 300 atmospheres. Nickel catalysts are widely used, including various types such as Raney nickel and nickel boride. The characteristic of precious metal platinum and palladium catalysts is high catalytic activity, and their dosage can be much less than nickel catalysts. When platinum is used as a catalyst, most of the ene bonds can be reduced under conditions below 100 ℃ and atmospheric pressure.
Most industries use platinum and palladium as carriers, and those using activated carbon as carriers are called platinum carbon and palladium carbon, respectively. Copper chromite Cu (CrO2) 2 has a low cost and is widely used in industry. Its characteristic is that it is particularly effective in catalyzing carbonyl groups, and has high catalytic ability for ester groups, amides, imides, etc. It has low activity for alkene and alkyne bonds, and is basically inactive for aromatic rings.

500l high-pressure hydrogenation kettlePurpose:;
Catalytic hydrogenation is suitable for large-scale and continuous production and has important industrial applications. For example, acetylene and propyne in petroleum cracking gas can be partially hydrogenated by palladium catalysis to produce high-purity ethylene and propylene. In the oil and fat industry, liquid oil is hydrogenated into solid or semi-solid fat to produce hardened oil for artificial butter or soap industry.
Palladium carbon is dissolved in ethanol and vacuum drawn into a high-pressure reactor or poured into the reactor. Then, ethanol is added to wash the container before being put into the reactor. After the reaction is complete, the material is filtered to recover palladium carbon. The reactor can be washed with reaction solvent and palladium carbon can be recovered through the filter.
(Hydrogenation reactor)500 liters | |||||||
serial number |
type |
specific parameters |
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1 |
model |
BR-500 |
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2 |
Cauldron body part |
(1)volume |
500 liters, open type, top flat cover and bottom head; |
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(2)pressure |
Inside the kettle |
jacket |
Inner coil tube |
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Work pressure(MPa) |
-0.1 ~ 0.5 |
0.6 |
0.4 |
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Design pressure(MPa) |
-0.1 ~ 5.0 |
0.8 |
0.6 |
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Maximum allowable(MPa) |
5.5 |
/ |
/ |
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(3) Temperature |
Inside the kettle |
jacket |
Inner coil tube |
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Working temperature(℃) |
-10 ~ 50 |
-10 ~ 50 |
-10 ~ 50 |
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Design temperature(℃) |
-30 ~ 150 |
-30 ~ 150 |
-30 ~ 150 |
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(4) Size |
Inside the kettle |
jacket |
Inner coil tube |
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Inner diameter(mm) |
800 |
950 |
Φ32 |
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Straight edge height(mm) |
950 |
950 |
/ |
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thickness |
Thickness(mm) |
3+20 |
8 |
/ |
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(5) Materials |
Inside the kettle |
jacket |
Boiler coil inside the kettle |
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working medium |
Methanol, isopropanol, hydrogen |
steam |
cooling water |
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medium characteristics |
Moderate hazard, explosive |
Non toxic, non flammable |
Non toxic, non flammable |
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Liquid receiving components |
S31603+16MnDR |
16MnDR |
S31603 |
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(6) Processing |
Internal surface polishing treatmentRa≤0.4μm, External surface painting; |
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3 |
stir system |
(1) Sealing |
Magnetic coupling seal, zero leakage |
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(2) Rotational speed |
motor |
YB7.5KwExplosion proof grade DIICT4, explosion-proof variable frequency motor |
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speed reducer |
TRXF88-YVB5.5-4P-3.78-M4, rotational speed300 revolutions per minute |
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(3) Paddle mixing |
Efficient self-priming (propulsion)+Self suction+disc turbine |
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4 |
equipment open one's mouth |
Upper discharge port |
DN32 |
With plug-in bottom tube |
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Solid feeding port |
DN65 |
With blind plate |
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rupture disc/Pressure gauge port |
DN40/15 |
Explosive fragments/Equipped with pressure gauge (digital display integrated, on-site display+remote transmission, range -0.1~1.0mpa, explosion-proof) |
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Vacuum exhaust port/Pressure gauge port |
DN25/15 |
Equipped with pressure gaugeIntegrated digital display, on-site display+remote transmission, range -0.1~1.0mpa, explosion-proof,accuracy class±0.1℃) |
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hydrogen import |
DN15 |
Equipped with bottom inserted hydrogen distributor |
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Liquid feed inlet |
DN25 |
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Temperature measuring port inside the kettle |
M27*2 |
Equipped with platinum resistance for temperature measurement (on-site display)+Remote transmission, explosion-proof level CT4) |
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Lower the clean mouth |
DN50 |
With blind blocking |
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Coil inlet |
DN20 |
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Coil outlet |
DN20 |
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Imported jacket |
DN40 |
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Jacket outlet |
DN40 |
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Jacket temperature measuring port |
M27*2 |
Equipped with platinum resistance for temperature measurement (on-site display)+Remote transmission, explosion-proof level CT4) |
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Jacket exhaust port |
M27*2 |
With blind blocking |
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(The opening of the equipment shall be subject to the final signed and confirmed drawings by both parties.) |
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5 |
other |
Other unconfirmed matters shall be subject to the signed and confirmed drawings by both parties. |
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