3L Automated Reactor

3L Automated Reactor

Beijing Century Senlang Pilot Test3L Automated ReactorIt is a large volume scientific research reaction equipment developed for the experimental amplification and pilot stage research. It integrates the excellent performance of AutoChen fully automatic reaction kettle and independent intellectual property SLMRSC-SLZ automation control system. The experiment realizes temperature and speed control, as well as temperature/speed/pressure/torque/timing data storage and acquisition. It can be configured with mobile remote operation control, intelligent configuration of floor structure, fixed kettle head and integrated design of the whole machine. The structure is reasonable, the functions are complete, and the Chinese menu is easy to use; Brand new touch screen operation; The kettle head is fixed and electrically lifted, equipped with a feeding structure or a flipping feeding system for easy experimental operation; The control system is equipped with dual temperature control modules (kettle and heater), automatic water inlet and cooling function, over temperature, over pressure and fault sound and light alarm function, constant temperature timing and programmed heating function, etc; A safer and more convenient robotic arm is used between the kettle body and the kettle cover, and the quick disassembly method of the snap ring facilitates the disassembly of the reaction kettle, improving work efficiency. Bottom discharge valve can be optionally selected to facilitate product recycling. Unlike desktop reactors, this floor standing stand can be equipped with various accessories such as condensers, solid feed ports, bottom temperature measurement ports, liquid feeding tanks, sample tanks with jackets, and solenoid valves, etc., to explore more possibilities and key process conditions for scaling up production.

pilot test3L Automated ReactorTechnical parameter description

1、 Host part

1.1 Reaction kettle, kettle head integral stirring system with electric lifting, stroke ranging from 400mm to 700mm

1.2 Full capacity: 3L

1.3 The kettle lid, kettle body material, and internal components are all made of 316L stainless steel material

1.4 Mixing driver, material: 316L stainless steel

1.5 composite high-temperature sealing gasket, quick opening snap ring seal, A-type double line sealing structure

1.6 Working pressure/temperature: 10MPa, 300 ℃

1.7 Heating furnace, self-developed high-temperature metal insulated heater, fast and stable temperature rise

1.8 Mixing speed control module and automatic cooling water control module

1.9 Pressure digital display and overpressure protection module, with pressure sensor

2、 Pilot Test3L Automated ReactorCauldron cover part

2.1 Dual range pointer pressure gauge and high-precision pressure transmitter

2.2 Safety explosion-proof valve

2.3 Thermowell and K-type thermocouple, used to measure the temperature of the reactor material, made of 316L stainless steel

2.4 Gas release valve, used to vent the gas inside the reaction kettle and release pressure, made of 316L stainless steel

2.5 Liquid feed valve, used for feeding, made of 316L stainless steel material

2.6 Built in cooling water coil, used for rapid cooling after the reaction is completed, made of 316L stainless steel

2.7 Magnetic coupling driven mechanical stirrer, equipped with four blade mold propeller (standard), made of 316L stainless steel

2.8 Direct mixing drive high torque motor: stepless speed regulation, controllable speed

IIIpilot test3L Automated ReactorControl section

3.1 Seven inch high brightness TFT LCD touch screen or laptop control system, with rich and comprehensive display content, no blind spots in the field of view
3.2 Identity recognition function, capable of graded control
3.3 Temperature digital display, dual channel internal and external temperature control monitoring function
3.4 Pressure digital display with ultra-high pressure protection function

3.5 Real time online curve display function for pressure, temperature, speed, torque, and alarm timing

3.6 Upgradeable to remote control function for mobile devices

3.7 Segmented program temperature control function, capable of setting multiple experimental condition heating modes, with a new AI artificial intelligence logic PID algorithm to achieve zero overshoot and overshoot control for complex and long lag objects

3.8 Automatic storage of experimental data, with built-in data recording function, can display real-time data, historical data, and provide report form recording data and alarm recording function.
3.9 Equipped with USB drive export function, it can be further analyzed and processed on the computer for long-term storage of experimental data for academic research papers.