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E-mail
tjjiaxinhai@163.com
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Phone
18002153016
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Address
No. 11 Guilin Road, Wudao Street, Heping District, Tianjin City - Negative 104-1029
Tianjin Jiaxinhai Machinery Equipment Co., Ltd
tjjiaxinhai@163.com
18002153016
No. 11 Guilin Road, Wudao Street, Heping District, Tianjin City - Negative 104-1029
In many fields such as modern material analysis, geological exploration, environmental monitoring, and scientific research, the demand for precise sample detection is increasing day by day. The fully automatic fluorescent tablet press, as an advanced equipment designed specifically for preparing high-quality and highly consistent fluorescent analysis samples, is playing a crucial role. It greatly improves the efficiency and quality of sample preparation with highly automated operation processes, precise pressure control, and excellent molding effects, laying a solid foundation for subsequent fluorescence spectroscopy analysis and other work.
1、 Working principle: Precise molding under intelligent control
(1) Mechanism of Pressure Generation and Transmission
Fully automatic fluorescent tablet presses are typically equipped with high-performance motors as power sources, which convert rotational motion into precise linear pressure through precision transmission devices such as ball screws or hydraulic systems. Taking ball screw transmission as an example, the high-speed rotation of the motor drives the screw to rotate, and the slider that cooperates with the screw moves linearly under the drive of the screw, thereby pushing the pressure head to apply pressure to the sample powder placed in the mold. This transmission method has the characteristics of high precision and high rigidity, which can ensure stable pressure output and precise control. The pressure is evenly transmitted to the sample powder inside the mold through the pressure head, generating strong squeezing force between the powder particles, promoting the particles to approach each other, fill the pores, and gradually form a tightly bonded sheet-like structure.
(2) Mixing and uniform distribution of fluorescent agents
During the sample compression process, if the addition of fluorescent agents is involved, there is a dedicated mixing system inside the equipment. The system adopts a unique stirring mechanism, such as a multi blade stirring blade or a planetary stirrer, which can efficiently mix the fluorescent agent with the sample powder. The shape, speed, and stirring time of the stirring blade are precisely controlled by the control system of the equipment to ensure uniform distribution of the fluorescent agent in the sample powder. For example, in geological sample analysis, in order to accurately detect mineral composition, specific fluorescent agents need to be thoroughly mixed with ground rock powder. The stirring blade is continuously stirred at a suitable speed (such as 200-300 revolutions per minute) for a certain period of time (about 3-5 minutes) to ensure that the fluorescent agent and rock powder are evenly mixed in the predetermined ratio, so that the pressed sample can present a stable and accurate fluorescence signal during fluorescence detection.
(3) Pressure control and regulation technology
The fully automatic fluorescent tablet press is equipped with an advanced pressure control system, which monitors the pressure value during the pressing process in real time through high-precision pressure sensors. The pressure sensor converts the collected pressure signal into an electrical signal and transmits it to the controller of the equipment. The controller adopts intelligent algorithms to accurately adjust the motor speed and torque based on preset pressure values and actual pressure feedback, achieving precise control of pressure. The operator can easily set the required parameters such as pressure magnitude, pressure rise rate, holding time, and pressure drop rate on the device's operating interface. For example, for some samples that are sensitive to pressure changes, a slow pressure rise rate (such as 0.1-0.2 MPa per second) can be set to avoid damage to the internal structure of the sample due to sudden pressure changes; During the holding phase, the controller can stabilize the pressure within a minimum error range of the preset value (such as ± 0.05MPa) to ensure sufficient densification of the sample; When reducing pressure, by precisely controlling the pressure reduction rate, cracks in the sample are prevented from occurring due to sudden pressure drops, ensuring the integrity and quality stability of the sample.
2、 Structural composition: Collaborative operation of precision components
(1) Power and transmission system
1. motorThe motor is the core power component of the fully automatic fluorescent tablet press. Depending on the performance requirements and application scenarios of the equipment, AC servo motors or DC brushless motors can be selected. AC servo motors have advantages such as high power density, high-precision control, and fast response, which can meet applications with high requirements for compression speed and pressure accuracy. For example, in large-scale material analysis laboratories, it is necessary to quickly and accurately prepare a large number of samples. AC servo motors can reach the set speed and torque in a short time, achieving efficient pressing processes. DC brushless motors have the characteristics of simple structure, high reliability, and easy maintenance, and are suitable for some cost sensitive and performance demanding occasions. The motor is connected to the transmission device through a coupling to ensure efficient transmission of power.
1. transmission deviceThe transmission device is responsible for converting the rotational motion of the motor into linear motion of the pressure head, and adjusting the motion speed and pressure as needed. Common transmission devices include ball screw transmission and hydraulic transmission. Ball screw transmission has the advantages of high transmission accuracy, high efficiency, and good rigidity. Ball rolling friction is used between the screw and nut, greatly reducing friction and improving transmission efficiency and accuracy. For example, in some research fields that require extremely high precision in sample compression, such as nanomaterial research, ball screw transmission can ensure that the positioning accuracy of the indenter reaches the micrometer level, thereby preparing samples with extremely high dimensional accuracy. Hydraulic transmission has the characteristics of high output force, smooth motion, and low noise, making it suitable for situations that require significant compression force. The hydraulic system delivers hydraulic oil to the hydraulic cylinder through an oil pump, which drives the piston to move the pressure head and generate a large pressure to meet the pressing requirements for samples with high hardness or large size.
(2) Pressure and Mold System
1. Pressure head and pressure sensorThe pressure head is a component that directly applies pressure to the sample, and its material and processing accuracy are crucial to the compression effect. The indenter is usually made of high-strength alloy steel, which has undergone precision machining and heat treatment. It has high surface hardness, good wear resistance, and can withstand enormous pressure. Pressure sensors are installed at critical parts of the pressure head or mold to monitor the pressure value in real-time during the pressing process. The accuracy and response speed of pressure sensors directly affect the accuracy and timeliness of pressure control. For example, using high-precision strain gauge pressure sensors, the measurement accuracy can reach ± 0.1% of the full range, which can quickly and accurately feedback pressure signals to the control system, ensuring that pressure control is within a very small error range.
1. mold componentsMold is a key component for achieving sample molding, usually consisting of an upper mold, a lower mold, and a middle mold. The design and manufacturing accuracy of molds directly affect the quality and dimensional accuracy of samples. The upper and lower molds are respectively connected to the pressure head and move towards each other under pressure, squeezing the sample powder placed in the middle mold. The middle mold plays a role in fixing the sample powder and guiding the movement of the pressure head, ensuring that the sample maintains the correct position and shape during the pressing process. The material of the mold is selected according to the characteristics of the pressed sample, generally using hard alloy or high-strength alloy steel to ensure that the mold has sufficient wear resistance, corrosion resistance, and compressive strength. In order to meet the needs of samples of different shapes and sizes, molds can be designed in various specifications, such as circular, square, irregular, etc., and can be easily replaced.
(3) Control System and Operating Interface
1. controllerThe controller is the core control unit of the fully automatic fluorescent tablet press, which adopts advanced programmable logic controller (PLC) or industrial computer (IPC). PLC has the advantages of high reliability, strong anti-interference ability, and simple programming, and is widely used in various industrial automation control systems. In the fully automatic fluorescent tablet press, PLC collects feedback signals from pressure sensors, displacement sensors, etc., and controls the start, stop, speed, and torque of the motor according to preset programs and parameters, achieving automated control of the pressing process. Industrial computers have powerful data processing capabilities and graphical interface display functions, enabling more complex control algorithms and human-computer interaction operations. For example, in some high-end fully automatic fluorescent tablet presses, industrial computers are used as controllers, which can collect and analyze a large amount of pressure, displacement, temperature and other data in real time, and optimize the pressing process through intelligent algorithms to improve the quality and efficiency of sample preparation.
1. operating interfaceThe operating interface usually adopts touch screen or industrial tablet computer, which has the characteristics of intuitive and convenient operation. The interface design conforms to the principles of ergonomics, and operators can easily complete device startup, shutdown, parameter settings, data queries, and other operations by touching the screen. Real time display of operating parameters such as pressure, displacement, temperature, and equipment status information on the interface, such as fault alarm prompts, facilitates operators to timely understand the equipment situation and take corresponding measures. At the same time, the operation interface also supports formula storage and calling functions. Operators can save commonly used pressing parameters as formulas and call them directly for the next use without resetting, greatly improving work efficiency. For example, in the geological sample analysis laboratory, operators can set and save corresponding compression formulas for different types of rock samples, which can be quickly called up in subsequent analysis to achieve efficient and accurate sample preparation.
3、 Technical advantage: Integration of efficiency, precision, and intelligence
(1) High degree of automation, improving work efficiency
The fully automatic fluorescent tablet press realizes the full process automation operation from sample powder filling, pressing, demolding to sample collection. The equipment is equipped with an automatic feeding system, such as a vibrating disc feeder or a spiral feeder, which can accurately control the filling amount of sample powder and evenly transport the powder to the mold. After the pressing is completed, the automatic demolding system can quickly and smoothly push the pressed sample out of the mold, and transport the sample to the collection device through a conveyor belt. The entire process does not require manual intervention, greatly reducing the time for sample preparation and improving work efficiency. For example, in environmental monitoring laboratories, it is necessary to analyze a large amount of soil, water samples, etc. The fully automatic fluorescent tablet press can prepare dozens or even hundreds of samples per hour. Compared with traditional manual tablet pressing methods, the work efficiency is several times or even tens of times higher, which can meet the needs of large-scale sample detection.
(2) Accurate pressure control ensures consistent sample quality
With advanced pressure control system and high-precision pressure sensors, the fully automatic fluorescent tablet press can achieve precise control of pressing pressure, with a pressure control accuracy of ± 0.05MPa or even higher. During the compression process, the equipment can operate strictly according to the preset pressure curve, ensuring that each sample can be compressed under the same pressure conditions. This precise pressure control ensures the consistency of physical properties such as density and hardness of the sample, thereby improving the accuracy and reliability of fluorescence analysis results. For example, in the process of material development, it is necessary to perform fluorescence analysis on samples from different batches to evaluate the stability of material performance. The fully automatic fluorescent tablet press can prepare samples with highly consistent quality, allowing the fluorescence analysis results to accurately reflect the true properties of the material and provide reliable data support for material research and development.
(3) Intelligent control and data analysis functions assist in process optimization
The control system of the fully automatic fluorescent tablet press has intelligent control and data analysis functions. The equipment can automatically adjust the motor speed, torque, and pressing time parameters based on preset parameters and actual pressing conditions, achieving optimization of the pressing process. At the same time, the control system can collect and store a large amount of compression data in real time, such as pressure, displacement, temperature, time, etc., and analyze and process these data to generate curves and reports of the compression process. By analyzing these data, operators can gain a deep understanding of various parameter changes during the pressing process, identify potential problems in a timely manner, and optimize the pressing process. For example, by analyzing the pressure curve, it is possible to determine whether there are problems such as uneven pressure and bubbles during the compression process of the sample, and adjust the compression parameters or improve the sample preparation process to improve the quality of the sample.
4、 Operation process: Simple and efficient standardized homework
(1) Preliminary preparation
1. Sample preparationPreprocess the compressed samples to ensure that their particle size, composition, etc. meet the process requirements. For solid samples, grinding, sieving and other operations are required to achieve the appropriate particle size range. Generally, the particle size of the sample powder is required to be between 100-200 mesh to ensure the fluidity and uniformity of the sample during the pressing process. For samples containing fluorescent agents, mix the fluorescent agent thoroughly with the sample powder according to the predetermined ratio.
1. Equipment inspectionCheck whether all components of the fully automatic fluorescent tablet press are intact, and whether the motor, transmission device, pressure sensor, etc. are working properly. Check if the mold is clean and undamaged, and if necessary, clean and maintain the mold. At the same time, check whether the lubrication system, cooling system, etc. of the equipment are operating normally to ensure that the equipment is working in good condition. For example, check whether there is residual sample powder on the surface of the mold, and if so, use a brush or compressed air to clean it; Check if the oil level of the lubrication system is within the normal range. If the oil level is insufficient, add lubricating oil in a timely manner.
(2) Parameter setting and operation
1. Parameter SettingsOn the operating interface of the device, set corresponding parameters based on the characteristics of the sample and the pressing requirements, such as pressure magnitude, pressure rise rate, holding time, pressure drop rate, filling amount, pressing times, etc. Operators can choose appropriate parameters based on experience or previous experimental results. At the same time, commonly used parameter combinations can be saved as formulas for easy access during the next use. For example, for a common geological sample, the pressure can be set to 20MPa, the pressure rise rate to 0.2MPa per second, the holding time to 30 seconds, the pressure drop rate to 0.1MPa per second, the filling amount to 5g, and the pressing times to 2.
1. start operationAfter setting the parameters, place the mold containing the sample powder in the designated position of the equipment, press the start button, and the equipment will automatically start running. The automatic feeding system precisely fills the sample powder into the mold, and then the pressure head applies pressure to the sample powder under the drive of the motor, pressing it according to the preset pressure curve. In
During the pressing process, the control system of the equipment monitors real-time parameters such as pressure and displacement, and adjusts them according to the actual situation to ensure the smooth progress of the pressing process.
(3) Sample extraction and equipment maintenance
1. Sample extractionAfter the pressing is completed, the automatic demolding system pushes the pressed sample out of the mold and transports it to the collection device through a conveyor belt. The operator carefully takes out the sample and checks the appearance quality of the sample, such as whether there are cracks, deformations, surface defects, etc. For samples with qualified appearance quality, subsequent fluorescence analysis and other testing work can be carried out; For non-conforming samples, analyze the reasons and adjust the parameters or prepare the samples again. ChineseEquipment maintenanceClean and maintain the equipment after use. Clean the residual sample powder on the surface of the equipment, molds, conveyor belts, and other parts to prevent powder accumulation from affecting the normal operation of the equipment. Check whether the various components of the equipment are worn, loose, etc. If so, repair or replace them in a timely manner. At the same time, maintain the lubrication system, cooling system, etc. of the equipment, add lubricating oil, replace coolant, etc., to ensure that the equipment is in good standby condition. For example, using a damp cloth to wipe the surface of the equipment, and using a brush to clean the residual powder inside the mold; Check if there is any looseness in the belt of the transmission device, and adjust it if necessary; Replace the coolant of the cooling system to ensure the heat dissipation effect of the equipment.
5、 Application areas: Sample preparation selection for multiple industries
(1) Geology and Mineral Industry
1. Mineral composition analysisIn geological exploration and mineral resource development, it is necessary to accurately analyze the composition and content of ores. The fully automatic fluorescent tablet press can mix and press the ground ore powder with fluorescent agent to prepare high-quality sample slices for X-ray fluorescence spectroscopy analysis. Through fluorescence analysis, the content of various elements in ores can be quickly and accurately determined, providing important basis for the evaluation of mineral resources and the optimization of mineral processing technology. For example, in the analysis of copper ore, samples prepared by a fully automated fluorescence compression machine can be accurately measured for the content of elements such as copper, iron, and sulfur using an X-ray fluorescence spectrometer, helping geologists determine the grade and mining value of the ore.
1. Rock researchGeologists need to conduct detailed analysis of rock samples when studying the genesis, evolution, and other processes of rocks. The fully automatic fluorescence tablet press can prepare rock sample slices that meet the requirements of fluorescence analysis. Through fluorescence detection of trace elements in rocks, the formation environment, geological history, and other information of rocks can be understood. For example, when studying volcanic rocks, analyzing the fluorescence characteristics of rare earth elements in samples can infer the nature of the volcanic eruption source area and the magma evolution process.
(2) Environmental monitoring field
1. Soil and water quality testingIn environmental monitoring, it is necessary to detect pollutants such as heavy metals and organic matter in soil and water samples. The fully automatic fluorescence tablet press can mix and compress soil samples or pre treated water samples with specific fluorescent reagents to prepare samples suitable for fluorescence analysis. Through fluorescence detection, the content of pollutants in soil and water can be quickly and accurately determined, providing data support for environmental quality assessment and pollution control. For example, when detecting the content of heavy metals such as lead and cadmium in soil, samples prepared using a fully automatic fluorescence compression machine can be quickly quantitatively analyzed for heavy metal content through a fluorescence spectrometer, and soil pollution problems can be detected in a timely manner.
1. Analysis of Atmospheric Particulate MatterThe fully automatic fluorescent tablet press also plays an important role in the analysis of chemical composition in atmospheric particulate matter. After processing the collected atmospheric particulate matter samples, they can be mixed and compressed with fluorescent agents to analyze the elemental composition, sources, and other information in the particulate matter. Fluorescence analysis of atmospheric particulate matter can help understand the causes and propagation patterns of air pollution, providing scientific basis for air pollution prevention and control.
(3) Materials Science and R&D
1. Research and development of new materialsIn the field of materials science, the development of new materials requires in-depth research on their properties. The fully automatic fluorescent tablet press can be used to prepare samples of various materials, such as ceramic materials, metal materials, polymer materials, etc., and to study the relationship between the structure, composition, and properties of materials through fluorescence analysis. For example, in the development of new luminescent materials, a fully automatic fluorescent tablet press is used to compress luminescent material powder into sample pieces. The luminescent characteristics are analyzed by fluorescence spectroscopy to optimize the formulation and preparation process of the material, thereby improving its luminescent efficiency and stability.
1. Material quality controlIn the process of material production, in order to ensure the stability of product quality, it is necessary to conduct quality testing on raw materials and finished products. The fully automatic fluorescent tablet press can prepare samples of consistent quality for fluorescence analysis and detection of impurity content, element distribution, and other indicators in materials, ensuring that the materials meet quality standards. For example, in the production of metal materials, fluorescence analysis of raw materials and finished product samples is used to detect the content of harmful elements and prevent the impact of excessive impurities on product quality.
The fully automatic fluorescent tablet press has become a key equipment in many industries such as modern material analysis due to its advanced working principle, precise structural composition, and wide application fields. With the continuous advancement of technology, fully automatic fluorescent tablet presses will develop towards higher levels of automation, higher pressure control accuracy, and more intelligent data processing, providing stronger technical support for innovative development in various industries and promoting the continuous improvement of research and production levels in related fields.