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What should be noted before, during, and after using a double-layer glass reactor
Date: 2025-11-17Read: 1
Jacketed Pilot Plant ReactorsUnder vacuum negative pressure conditions, the principle of constant temperature heating and constant speed stirring is used to uniformly stir the raw materials, allowing them to fully react, evaporate, separate, and recover solvents in the kettle. All parts in contact with the materials are made of high temperature resistant and corrosion-resistant borosilicate glass and polytetrafluoroethylene materials, which are suitable for the reaction of easily decomposed and denatured biological products and are not prone to chemical reactions with various materials.
Main functions and application scenarios:
Chemical reactions: suitable for organic synthesis, drug preparation, material research and development, etc., supporting high temperature, high pressure, and high vacuum conditions.
Separation and purification: used for solvent recovery, distillation, extraction and other operations, especially suitable for mild reactions that require visual monitoring.
Multi domain applications: widely used in scientific research and teaching in fields such as chemistry, pharmaceuticals, food, and chemical engineering.
Pre use inspection:
Check whether there are cracks, scratches or damage on the glass components (kettle body, interlayer, inner wall), and whether the sealing surface is flat.
Confirm that the sealing ring is intact, apply vacuum silicone grease during installation to enhance sealing, and gradually tighten the clips in diagonal order.
Ensure that the mixing blade is installed in the center, rotates flexibly, and all interfaces are firmly connected.
Check the level of thermal oil and strictly prohibit dry burning; Confirm that the cooling water pressure is normal.
Empty load test run, observe whether the mixing is smooth and whether there is any leakage.
Precautions during use:
Temperature control should be gradual to avoid sudden cooling and heating that may cause glass breakage.
Wear goggles and gloves throughout the entire process, and immediately turn off the power after stopping.
Real time monitoring of temperature, pressure and other parameters, and timely handling of any abnormalities.
After use operation:
Immediately clean the reaction kettle to prevent residue from drying out.
Turn off the power and medium valves, and clean the inside and outside of the equipment.