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Shanghai Qiangqiang Industrial Development Co., Ltd

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Operating the glass reactor in this way can make you twice as efficient with half the effort
Date: 2017-08-10Read: 1
The inner tank of a double-layer glass reactor is filled with reaction materials and stirred under normal or negative pressure in a closed state. The interlayer can be connected to a medium (frozen liquid, heated water or heated oil) for circulating heating or cooling. The double-layer glass reactor (motor adopts fully explosion-proof motor, electrical appliances adopt explosion-proof electrical box, cabinet and local safety chemical explosion-proof treatment) greatly meets the explosion-proof requirements of modern biological, chemical, pharmaceutical and other experimental production workshops, achievingQ/HA01—2005Standard.

The following mainly discusses how to better operate the instrument:

1.If there is abnormal noise inside the isolation sleeve during operation, the machine should be stopped to release pressure and the mixing system should be checked for any abnormal conditions. Regularly check the swing amount of the mixing shaft. If the swing amount is too large, the bearing or sliding shaft sleeve should be replaced in a timely manner.

2.When conducting reactions with different media in a glass reactor, it is necessary to first investigate whether the media corrode the main material. Special orders are required for chemical reactions that cause rapid reactions, generate large amounts of gas, or are flammable and explosive at high temperatures, as well as reactions that corrode stainless steel severely due to high pressure, high temperature, or the presence of chloride and fluoride ions in the medium. Except for the transparent glass of the kettle body and jacket, all others are made of stainless steel or other metal materials.

3.When heating the jacket heat transfer oil, be careful not to mix water or other liquids into it. The oil level of the heat transfer oil should be checked periodically.

4.After the final reaction temperature is determined, it is not allowed to change the temperature setting during the heating process to avoid significant temperature overshoot.

5.When loading the reaction medium, it should not exceed the kettle body2/3liquid surface.

6.It is strictly prohibited to disassemble under pressure during or after work!It is strictly prohibited for the kettle to work under overpressure or overheating conditions.