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Shandong Ruineng Instrument Co., Ltd
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instrumentb2b>Solution>Gas chromatograph for photocatalytic detection of CO2 reduction reaction
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Shandong Ruineng Instrument Co., Ltd

  • E-mail

    sdrnyq@163.com

  • Phone

    13656375202

  • Address

    No. 2828, Parallel North Road, Tengzhou City, Shandong Province

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▏Product Features

The GC3900Pro gas chromatograph is a professional version (performance version) with a 7-inch touch screen and stable voltage regulationFlow control flow path, optional(EPC Electronics

Flow and pressure control system, pressure and flow digital display function, abandoning mechanical display of pressure gauge), digital circuit,IP communication technology, bus technology, network transmission,

Digital quantity 485 transmission, realizing chromatographyInstrument online analysis, capable of remote control, etc., can be installed at mostThree types of detectors


▏Test Principle


Gas chromatograph is a separation and analysis tool for multi-component mixtures, which uses inert gas as the mobile phase and employs chromatographic column separation technology. When there are multiple fractions

When the analyte enters the chromatographic column, due to the different distribution coefficients of each component in the column, the flow velocities of each component in the column are different. After a certain period of

After the column length, the mixed components leave the chromatography column and enter the detector. After detection, they are converted into electrical signals and sent to the data processing workstation to complete the measurement of the tested components

Detection and analysis of substances.


▏Test application


Basic Application

CO2

Photocatalytic detection of CO2 reduction reaction

▏Technical Specifications

indicator

parameter

Temperature of chromatographic column chamber

Temperature control range: room temperature ± 8 ℃ -450 ℃, with increments of 1 ℃

Temperature control accuracy: ± 0.1 ℃ - ± 0.2 ℃

Temperature control area: 6-way temperature control

Program heating order

16th order

heating rate

0.1-40 ℃/min, with increments of 0.1 ℃, initial and termination times

Range: 0-6000min, with increments of 1min

Pressure protection method

The carrier gas has pressure protection function, and the gas pressure is lower than

At 0.1MPa, the instrument automatically cuts off the power supply, effectively protecting the color

Safe use of spectral columns

display mode

7-inch touchscreen LCD display

Extreme temperature

Maximum protection value 450 ℃

external event

8通道外部事件

Hydrogen flame ionization detector (FID)

Ignition method: automatic ignition

Mt≤5×10-12g/s(n-Hexadecane-Isooctane Solution)

Noise:≤1×10-14A

Drift:1×10-13A/30min

Linear range: ≥ 106

power supply

220V 50HZ 2000W

▏Product Configuration

Instrument model

GC3900Pro (this instrument has automatic ignition function)

quantity

1 unit

analyze samples

Reactive gas

Sample components

H2TheO2TheN2TheCOTheCO2TheCH4TheC2H6TheC2H4TheC2H2Alcohols and acidsanalyze

configuration

Specification Model

quantity

host

GC3900Pro

Room temperature ± 8 ℃ -450 ℃, in increments of 1 ℃

Temperature control accuracy: ± 0.1 ℃ - ± 0.2 ℃

Temperature gradient: ± 1%

16 stage program heating, heating rate 0.1-40 ℃/min, in increments of 0.1 ℃,

Initial and termination time range: 0-6000min, with increments of 1min.

Extreme temperature: maximum protection value 450 ℃

Injection system Capillary column injection system

Injection system

Fill column injection system

1 set

detector

thermal conductivityDetector (TCD)

Sensitivity S ≥ 5000mV · ml/mg

1 piece

Noise ≤ 20 μ V

Drift ≤ 30 μ V/15 min

workstation

Dedicated Workstation

1 set

chromatographic column

Capillary chromatography column

PQ column, GDX-502 column, 5A column

3 pieces

gas source

nitrogen cylinder

99.999% high-purity nitrogen with pressure reducing valve (self equipped)

1 bottle

Computer, printer

Computer, printer

Win7/ win10

1 set

▏analysis process

1analyzeH2O2、N2TheCO、CO2TheCH4TheC2H6、C2H4TheC2H2

图片1(1)(1).png

After the sample enters column 1 through valve 1, after the gas flows out of column 1, valve 1 switches to blow back alcohols, acids, etc. Column 2 separates C1 and C2. Among them, C1 is H2, O2

N2, CO, CH4 peak combination. After entering column 3, valve 2 switches. CO2 and C2 enter TCD through damping and then enter FID II through valve 3. Analyze C2H6

Content of C2H4 and C2H2. After C2 is completed, valve 2 is reset. Column 3 separates H2, O2, N2, CO, and CH4 into TCD. Detect H2, O2, N2, continue

Entering valve 3 (switching valve 3), it enters the converter, where CO is converted into CH4. Upon entering FID II, CO and CH4 are detected.

Note: Due toTCDLimited sensitivity,H2TheO2TheN2If the concentration is too low, it may not be detectable.

2、 Instrument and equipment


The gas chromatograph should be equipped with a thermal conductivity detector (TCD) and a hydrogen flame ionization detector (FID), gas six way valve, ten way valve, and solenoid valve

▏Spectral analysis results


CO2光催化).png